Spectra for:
David J. Edmonds, Kenneth W. Muir, David J. Procter
Compound 8A (3S,4S)-3-[(1S)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4-HYDROXY-4,5-DIHYDROFURAN-2(3H)-ONE
![(3S,4S)-3-[(1S)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4-HYDROXY-4,5-DIHYDROFURAN-2(3H)-ONE](/api/compound/81HZeshdpxL.png?h=300&w=458 "(3S,4S)-3-[(1S)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4-HYDROXY-4,5-DIHYDROFURAN-2(3H)-ONE")
Compound 8B (3S,4S)-3-[(1R)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4-HYDROXY-4,5-DIHYDROFURAN-2(3H)-ONE
![(3S,4S)-3-[(1R)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4-HYDROXY-4,5-DIHYDROFURAN-2(3H)-ONE](/api/compound/98j7cVFvrUm.png?h=300&w=458 "(3S,4S)-3-[(1R)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4-HYDROXY-4,5-DIHYDROFURAN-2(3H)-ONE")
Compound 9A (3S,4S)-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[(1S)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4,5-DIHYDROFURAN-2(3H)-ONE
![(3S,4S)-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[(1S)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4,5-DIHYDROFURAN-2(3H)-ONE](/api/compound/2oY3ZqWFTmt.png?h=300&w=458 "(3S,4S)-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[(1S)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4,5-DIHYDROFURAN-2(3H)-ONE")
Compound 9B (3S,4S)-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[(1R)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4,5-DIHYDROFURAN-2(3H)-ONE
![(3S,4S)-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[(1R)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4,5-DIHYDROFURAN-2(3H)-ONE](/api/compound/HPyx55Sbrgu.png?h=300&w=458 "(3S,4S)-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[(1R)-3-([1,3]-DITHIAN-2-YL)-1-HYDROXY-3-METHYLBUTYL]-4,5-DIHYDROFURAN-2(3H)-ONE")
Compound 10 (4S)-E-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE
![(4S)-E-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE](/api/compound/GYnmZdBUgIp.png?h=300&w=458 "(4S)-E-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE")
Compound 11 (4S)-Z-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE
![(4S)-Z-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE](/api/compound/7KlASXOom9u.png?h=300&w=458 "(4S)-Z-4-TERT.-BUTYLDIMETHYLSILYLOXY-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE")
Compound 12 E-4-[(4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL
![E-4-[(4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL](/api/compound/C6H8lRXWunf.png?h=300&w=458 "E-4-[(4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL")
Compound 13 (3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
![(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE](/api/compound/HPMDwbfZaTT.png?h=300&w=458 "(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE")
Compound 13-EPI (3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
![(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE](/api/compound/FZ1zrD6l2am.png?h=300&w=458 "(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE")
Compound 15 (3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S,2S)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
![(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S,2S)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE](/api/compound/7XQ3VC0ylmd.png?h=300&w=458 "(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S,2S)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE")
Compound 16 (4S)-E-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4-HYDROXY-4,5-DIHYDROFURAN-2-ONE
![(4S)-E-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4-HYDROXY-4,5-DIHYDROFURAN-2-ONE](/api/compound/FGATH7ASCem.png?h=300&w=458 "(4S)-E-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4-HYDROXY-4,5-DIHYDROFURAN-2-ONE")
Compound 17 (4S)-E-4-(TERT.-BUTYL.-DIPHENYLSILYLOXY)-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE
![(4S)-E-4-(TERT.-BUTYL.-DIPHENYLSILYLOXY)-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE](/api/compound/1LpYR41wxES.png?h=300&w=458 "(4S)-E-4-(TERT.-BUTYL.-DIPHENYLSILYLOXY)-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4,5-DIHYDROFURAN-2-ONE")
Compound 18 E-4-[(4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL
![E-4-[(4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL](/api/compound/3QkQpdT1zHX.png?h=300&w=458 "E-4-[(4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL")
Compound 19 (4S)-E-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4-METHOXYMETHOXY-4,5-DIHYDROFURAN-2-ONE
![(4S)-E-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4-METHOXYMETHOXY-4,5-DIHYDROFURAN-2-ONE](/api/compound/JtHXTGPgQEx.png?h=300&w=458 "(4S)-E-3-[3-([1,3]-DITHIAN-2-YL)-3-METHYLBUTYLIDENE]-4-METHOXYMETHOXY-4,5-DIHYDROFURAN-2-ONE")
Compound 20 E-4-[(4S)-4-METHOXYMETHOXY-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL
![E-4-[(4S)-4-METHOXYMETHOXY-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL](/api/compound/LYJk3DizZck.png?h=300&w=458 "E-4-[(4S)-4-METHOXYMETHOXY-2-OXO-4,5-DIHYDROFURAN-3-YLIDENE]-2,2-DIMETHYLBUTANAL")
Compound 21 (3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R)-3,3-DIMETHYL-2-OXOCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
![(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R)-3,3-DIMETHYL-2-OXOCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE](/api/compound/LKbomgkVWZH.png?h=300&w=458 "(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R)-3,3-DIMETHYL-2-OXOCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE")
Compound 22 (1S,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-HYDROXYETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE
![(1S,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-HYDROXYETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE](/api/compound/7OxC5PHdQmz.png?h=300&w=458 "(1S,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-HYDROXYETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE")
Compound 23 (3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S)-3,3-DIMETHYL-2-OXA-CYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
![(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S)-3,3-DIMETHYL-2-OXA-CYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE](/api/compound/8UTEtKTKdT2.png?h=300&w=458 "(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S)-3,3-DIMETHYL-2-OXA-CYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE")
Compound 24 (1S,4R,5S)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-HYDROXYETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE
![(1S,4R,5S)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-HYDROXYETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE](/api/compound/Vj58sg31aS.png?h=300&w=458 "(1S,4R,5S)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-HYDROXYETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE")
Compound 25 (1S,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-(TRIETHYLSILYLOXY)-ETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE
![(1S,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-(TRIETHYLSILYLOXY)-ETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE](/api/compound/7avAygBjWRE.png?h=300&w=458 "(1S,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-(TRIETHYLSILYLOXY)-ETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-ONE")
#26;(1S,3R,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-(TRIETHYLSILYLOXY)-ETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-OL;MAJOR-ISOMER
![#26;(1S,3R,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-(TRIETHYLSILYLOXY)-ETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-OL;MAJOR-ISOMER](/api/compound/JNfTdZEN8nX.png?h=300&w=458 "#26;(1S,3R,4S,5R)-4-[(1S)-1-(TERT.-BUTYLDIMETHYLSILYLOXY)-2-(TRIETHYLSILYLOXY)-ETHYL]-7,7-DIMETHYL-1-VINYL-2-OXABICYCLO-[3.2.0]-HEPTAN-3-OL;MAJOR-ISOMER")
Citation
| Citation | J.ORG.CHEM.,68,3190(2003) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 8 |
| Volume | 68 |
| Page(s) | 3190-3198 |
| Year | 2003 |
| Author(s) | David J. Edmonds, Kenneth W. Muir, David J. Procter |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo026827o |