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(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE

Compound with spectra: 1 NMR, and 1 MS (GC)

(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
SpectraBase Compound ID HPMDwbfZaTT
InChI InChI=1S/C16H30O4Si/c1-15(2,3)21(6,7)20-11-9-19-14(18)12(11)10-8-16(4,5)13(10)17/h10-13,17H,8-9H2,1-7H3/t10-,11-,12+,13-/m1/s1
InChIKey QUGDVUNCLJHOLV-FVCCEPFGSA-N
Mol Weight 314.5 g/mol
Molecular Formula C16H30O4Si
Exact Mass 314.191336 g/mol
Enantiomer InChIKey QUGDVUNCLJHOLV-RVMXOQNASA-N

View Spectrum of (3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE

MS (GC) Spectrum
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Source of Spectrum F-68-3195-13

View Spectrum of (3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • (3S,4S)-4-[tert-butyl(dimethyl)silyl]oxy-3-[(1R,2R)-2-hydroxy-3,3-dimethyl-cyclobutyl]tetrahydrofuran-2-one
(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R,2R)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S,2S)-2-HYDROXY-3,3-DIMETHYLCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
(3S,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1R)-3,3-DIMETHYL-2-OXOCYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
(3R,4S)-4-(TERT.-BUTYLDIMETHYLSILYLOXY)-3-[(1S)-3,3-DIMETHYL-2-OXA-CYCLOBUTYL]-4,5-DHYDROFURAN-2(3H)-ONE
(2R)-2-[tert-butyl(dimethyl)silyl]oxy-2-[(1R,2S,3S,5R)-3-hydroxy-2-methyl-5-(1-methylethenyl)cyclohexyl]acetic acid methyl ester
(2R*,1'R*,2'S*,3'S*,5'R*)-2-[5'-Acetoxy-3'-hydroxy-2'-methylenecyclohexyl)-2-tert-butyldimethylsilyloxyacetic acid methyl ester
(1R,1'R,2R,3S,6S)-{[6-{2'-{[Dimethyl(1,1,2-trimethylpropyl)silyl]oxy}-1'-methylethyl}-2,3-epoxy-3-methylcyclohexyl]oxy}trimethylsilane
(1S,1'S,2R,3S,6S)-{[6-{2'-{[Dimethyl(1,1,2-trimethylpropyl)silyl]oxy}-1'-methylethyl}-2,3-epoxy-3-methylcyclohexyl]oxy}trimethylsilane
(1S,4aR,8S,8aS)-8-[tert-butyl(dimethyl)silyl]oxy-1,2,4a,5,6,7,8,8a-octahydronaphthalene-1-carboxylic acid methyl ester
(1S,2S,3R,4S)-4-(tert-Butyldimethylsilanyloxy)-3-(tert-butyldimethylsilanyloxymethyl)-2-chloromethylcyclopentanecarboxylic acid acid methyl ester
Title Journal or Book Year
The Remarkable Effect of Cosolvent on a Samarium(II)-Mediated 4-exo-trig Cyclization:  Further Synthetic Studies on Pestalotiopsin A The Journal of Organic Chemistry 2003
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