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5-ENDO-([(TERT.-BUTYLDIMETHYLSILYL)-OXY]-METHYL)-4-(4''-METHYLBENZENESULFENYL)-2-(4'-METHYLBENZENESULFONYL)-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE

Compound with spectra: 1 NMR

5-ENDO-([(TERT.-BUTYLDIMETHYLSILYL)-OXY]-METHYL)-4-(4''-METHYLBENZENESULFENYL)-2-(4'-METHYLBENZENESULFONYL)-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE
SpectraBase Compound ID FgVhgZLggZT
InChI InChI=1S/C28H37NO4S2Si/c1-20-8-12-24(13-9-20)34-28-17-16-23(18-22(28)19-33-36(6,7)27(3,4)5)29(26(28)30)35(31,32)25-14-10-21(2)11-15-25/h8-17,22-23H,18-19H2,1-7H3/t22-,23+,28+/m1/s1
InChIKey SIOYKGPXFNWVES-IWHLBADBSA-N
Mol Weight 543.8 g/mol
Molecular Formula C28H37NO4S2Si
Exact Mass 543.193328 g/mol
Enantiomer InChIKey SIOYKGPXFNWVES-SXDGJLEOSA-N

View Spectrum of 5-ENDO-([(TERT.-BUTYLDIMETHYLSILYL)-OXY]-METHYL)-4-(4''-METHYLBENZENESULFENYL)-2-(4'-METHYLBENZENESULFONYL)-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
5-endo-[[(Butyldimethylsilyl)oxy]methyl]-4-(4"-Methylbenzenesulfenyl)-2-(4'-methylbenzenesulfonyl)-3-oxo-2-azabicyclo[2.2.2]-7-octene
4-(4''-METHYLBENZENESULFENYL)-2-(4'-METHYLBENZENESULFONYL)-5-EXO-NITRO-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE
4-(4"-Methylbenzenesulfenyl)-2-(4'-methylbenzenesulfonyl)-5-endo-nitro-3-oxo-2-azabicyclo[2.2.2]-7-octene
4-(4''-METHYLBENZENESULFENYL)-2-(4'-METHYLBENZENESULFONYL)-5-ENDO-NITRO-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE
4-(BENZYLOXY)-5-ENDO-([(TERT.-BUTYLDIMETHYLSILYL)-OXY]-METHYL)-2-(4'-METHYLBENZENESULFONYL)-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE
4-(Benzyloxy)-5-endo-[(tert-butyldimethylsilyloxy)methyl]-2-(4'-methylbenzenesulfonyl)-3-oxo-2-azabicyclo[2.2.2]-7-octene
4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-2-(4'-METHYLBENZENESULFONYL)-5-ENDO-NITRO-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE
4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-2-(4'-METHYLBENZENESULFONYL)-3-OXO-2-AZABICYCLO-[2.2.2]-OCT-7-ENE-5-ENDO-CARBOXALDEHYDE
4-([tert-Butyldimethylsilyl)oxy]-2-(4'-Methylbenzenesulfonyl)-3-oxo-2-azabicyclo[2.2.2]-7-octene-5-endo-carboxadehyde
Dimethyl 2-(bromomethyl)-2-phenyl-2H,9aH-pyrido[2,1-b][1,3]oxazine-3,4-dicarboxylate
Title Journal or Book Year
Diels-Alder cycloadditions using nucleophilic 2-pyridones. Regiocontrolled and stereocontrolled synthesis of unsaturated, bridged, bicyclic lactams The Journal of Organic Chemistry 1992
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