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(SYN)-1-[(4S,5R)-5-[(S)-2-(TERT.-BUTYLDIPHENYLSILYLOXY)-3-METHYLBUTYL]-2-PHENYL-1,3,2-DIOXABOROLAN-4-YL]-ETHANONE;MAJOR-DIASTEREOMER

Compound with spectra: 1 NMR

(SYN)-1-[(4S,5R)-5-[(S)-2-(TERT.-BUTYLDIPHENYLSILYLOXY)-3-METHYLBUTYL]-2-PHENYL-1,3,2-DIOXABOROLAN-4-YL]-ETHANONE;MAJOR-DIASTEREOMER
SpectraBase Compound ID 6QzPMS8mAgn
InChI InChI=1S/C31H39BO4Si/c1-23(2)28(22-29-30(24(3)33)35-32(34-29)25-16-10-7-11-17-25)36-37(31(4,5)6,26-18-12-8-13-19-26)27-20-14-9-15-21-27/h7-21,23,28-30H,22H2,1-6H3/t28-,29+,30+/m0/s1
InChIKey HMVVBYZISLNQLT-FRXPANAUSA-N
Mol Weight 514.5 g/mol
Molecular Formula C31H39BO4Si
Exact Mass 514.271066 g/mol
Enantiomer InChIKey HMVVBYZISLNQLT-NGDRWEMDSA-N

View Spectrum of (SYN)-1-[(4S,5R)-5-[(S)-2-(TERT.-BUTYLDIPHENYLSILYLOXY)-3-METHYLBUTYL]-2-PHENYL-1,3,2-DIOXABOROLAN-4-YL]-ETHANONE;MAJOR-DIASTEREOMER

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
(ANTI)-1-[(4R,5S)-5-[(S)-2-(TERT.-BUTYLDIPHENYLSILYLOXY)-3-METHYLBUTYL]-2-PHENYL-1,3,2-DIOXABOROLAN-4-YL]-ETHANONE;MAJOR-DIASTEREOMER
(1R,3AS,4R,5R,6AS)-5-[[TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-1,4-DIMETHYLHEXAHYDROPENTALEN-2(1H)-ONE
(3AS,4R,5R,6AR)-4-ALLYL-5-[(TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-HEXAHYDROPENTALEN-2(1H)-ONE
[(1R,2S,3S)-3-TERT.-BUTYLDIPHENYLSILYLOXY-2-[(4S)-2,2-DIMETHYL-1,3-DIOXOLAN-4-YL]:CYCLOBUTYL]-METHANOL
(1S,3AR,5R,6R,6AS)-5-[[TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-1,6-DIMETHYLHEXAHYDROPENTALEN-2(1H)-ONE
(3AR,5R,6R,6AS)-6-ALLYL-5-[[TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-1,3A,4,5,6,6A-HEXAHYDROPENTALEN-1-OL
METHYL-4-O-BENZOYL-2-O-TERT.-BUTYLDIPHENYLSILYL-3,6-DIDEOXY-ALPHA-D-ARABINO-HEXOPYRANOSIDE
(5R)-5-[tert-butyl(diphenyl)silyl]oxy-5-[(1S,2R)-2-[(E)-2-[(4R,5S)-2,2-dimethyl-5-[(Z)-oct-2-enyl]-1,3-dioxolan-4-yl]ethenyl]cyclopropyl]pentanoic acid methyl ester
(1'E,6'Z)-(1S,2R,3'S,4'S,1''R)-1-(5'-tert-Butyldimethylsilyloxy-1'-tert-butyldiphenylsiloxypentyl)-2-(3',4'-dihydroxy-3',4'-O-isopropylideneundec-1',6'-dienyl)cyclopropane
(4R,5R)-2,2-Dimethyl-4-(tert-Butyldimethylsiloxymethyl)-5-[1-(tert-butyldiphenylsilyloxy)butyl][1,3]dioxolane
Title Journal or Book Year
Stereocontrolled Synthesis of 1,3,5-Triols by an Iteration of Asymmetric Dihydroxylation and Deoxygenation European Journal of Organic Chemistry 2010
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