Spectra for:
Antonio Abad, Consuelo Agulló, Manuel Arnó, Ana C. Cuñat, Benjamín Meseguer, Ramón J. Zaragozá
Compound 1 STYPODIOL;(3-BETA,5-ALPHA,13-ALPHA)-14,17-EPOXY-4,4,8-TRIMETHYL-16,24-CYCLO-13,17-SECOCHOLA-16,20(22),23-TRIENE-3,23-DIOL
Compound 2 EPISTYPODIOL;(3-BETA,5-ALPHA,13-ALPHA,14-BETA)-14,17-EPOXY-4,4,8-TRIMETHYL-16,24-CYCLO-13,17-SECOCHOLA-16,20(22),23-TRIENE-3,23-DIOL
Compound 8 HDVXRNIZHQRLBD-UWVGGRQHSA-N
Compound 8 (5R,6R)-2,6-DIMETHYL-5-(1-METHYLETHENYL)-2-CYCLOHEXEN-1-ONE
Compound 9 (5R,6R)-6-(3,3-Diethoxypropyl)-2,6-dimethyl-5-(1-methylethenyl)-2-cyclohexen-1-one
Compound 10 3-[(1R,6R)-1,3-DIMETHYL-6-(1-METHYLETHENYL)-2-OXO-3-CYCLOHEXENYL]-1-PROPANOL
![3-[(1R,6R)-1,3-DIMETHYL-6-(1-METHYLETHENYL)-2-OXO-3-CYCLOHEXENYL]-1-PROPANOL](/api/compound/HBRiKkPAaNy.png?h=300&w=458 "3-[(1R,6R)-1,3-DIMETHYL-6-(1-METHYLETHENYL)-2-OXO-3-CYCLOHEXENYL]-1-PROPANOL")
Compound 11 (5R,6R)-2,6-Dimethyl-5-(1-methylethenyl)-6-[(E)-4-methyl-5-oxo-3-hexenyl]-2-cyclohexen-1-one
![(5R,6R)-2,6-Dimethyl-5-(1-methylethenyl)-6-[(E)-4-methyl-5-oxo-3-hexenyl]-2-cyclohexen-1-one](/api/compound/CTUUn2d9hFL.png?h=300&w=458 "(5R,6R)-2,6-Dimethyl-5-(1-methylethenyl)-6-[(E)-4-methyl-5-oxo-3-hexenyl]-2-cyclohexen-1-one")
Compound 12 2,6-DIMETHYL-5-(1-METHYLETHENYL)-6-[(E)-4-METHYL-5-OXO-3-HEXENYL]-2-CYCLOHEXEN-1-ONE
![2,6-DIMETHYL-5-(1-METHYLETHENYL)-6-[(E)-4-METHYL-5-OXO-3-HEXENYL]-2-CYCLOHEXEN-1-ONE](/api/compound/LU8h3uCcc6S.png?h=300&w=458 "2,6-DIMETHYL-5-(1-METHYLETHENYL)-6-[(E)-4-METHYL-5-OXO-3-HEXENYL]-2-CYCLOHEXEN-1-ONE")
Compound 13 (5R,6R)-6-[(3-E)-5-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-METHYL-3,5-HEXADIENYL]-2,6-DIMETHYL-5-(1-METHYLETHENYL)-2-CYCLOHEXEN-1-ONE
![(5R,6R)-6-[(3-E)-5-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-METHYL-3,5-HEXADIENYL]-2,6-DIMETHYL-5-(1-METHYLETHENYL)-2-CYCLOHEXEN-1-ONE](/api/compound/K3C6Wz3PZqh.png?h=300&w=458 "(5R,6R)-6-[(3-E)-5-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-METHYL-3,5-HEXADIENYL]-2,6-DIMETHYL-5-(1-METHYLETHENYL)-2-CYCLOHEXEN-1-ONE")
Compound 14 [4AR-(4A-ALPHA,4B-BETA,8-BETA,8A-ALPHA,10A-BETA)]-4A,4B,5,6,7,8,8A,9,10,10A-DECAHYDRO-2,4B,8,10A-TETRAMETHYL-7-OXO-1-(4H)-PHENANTHRENONE
![[4AR-(4A-ALPHA,4B-BETA,8-BETA,8A-ALPHA,10A-BETA)]-4A,4B,5,6,7,8,8A,9,10,10A-DECAHYDRO-2,4B,8,10A-TETRAMETHYL-7-OXO-1-(4H)-PHENANTHRENONE](/api/compound/9ogdmyms4ZI.png?h=300&w=458 "[4AR-(4A-ALPHA,4B-BETA,8-BETA,8A-ALPHA,10A-BETA)]-4A,4B,5,6,7,8,8A,9,10,10A-DECAHYDRO-2,4B,8,10A-TETRAMETHYL-7-OXO-1-(4H)-PHENANTHRENONE")
Compound 22 (5.alpha.,13.alpha.)-14,17-Epoxy-23-hydroxy-4,4,8-trimethyl-16,24-cyclo-13,17-secochola-16,20(22)-23-trien-3-one
Compound 25 (5-ALPHA,13-ALPHA,14-BETA)-14,17-EPOXY-23-HYDROXY-4,4,8-TRIMETHYL-16,24-CYCLO-13,17-SECOCHOLA-16,20(22),23-TRIEN-3-ONE
#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA
![#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA](/api/compound/7Zh5iwtABQk.png?h=300&w=458 "#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA")
#16;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-TETRADECAHYDRO-1A,3A,5,7B-TETRAMETHYL-4-H-CYCLOPROP
![#16;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-TETRADECAHYDRO-1A,3A,5,7B-TETRAMETHYL-4-H-CYCLOPROP](/api/compound/JJkPvxRVAcj.png?h=300&w=458 "#16;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-TETRADECAHYDRO-1A,3A,5,7B-TETRAMETHYL-4-H-CYCLOPROP")
#18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL
![#18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL](/api/compound/JAEoVv7KTo2.png?h=300&w=458 "#18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL")
#19;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-BETA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL]
![#19;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-BETA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL]](/api/compound/CxhWgJVc9CP.png?h=300&w=458 "#19;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-BETA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL]")
#6;[4AR-(4A-ALPHA,4B-BETA,8A-ALPHA,10A-BETA)]-7-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-2,4B,8,10A-TETRAMETHYL-4A,4B,5,6,8A,9,10,10A-OCTAHYDRO-1-(4H)-PHENANTHRENONE
![#6;[4AR-(4A-ALPHA,4B-BETA,8A-ALPHA,10A-BETA)]-7-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-2,4B,8,10A-TETRAMETHYL-4A,4B,5,6,8A,9,10,10A-OCTAHYDRO-1-(4H)-PHENANTHRENONE](/api/compound/KJMXW0OkwuF.png?h=300&w=458 "#6;[4AR-(4A-ALPHA,4B-BETA,8A-ALPHA,10A-BETA)]-7-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-2,4B,8,10A-TETRAMETHYL-4A,4B,5,6,8A,9,10,10A-OCTAHYDRO-1-(4H)-PHENANTHRENONE")
3-IODOPROPANALDEHYDE-DIETHYLACETAL
Citation
| Citation | J.ORG.CHEM.,63,5100(1998) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 15 |
| Volume | 63 |
| Page(s) | 5100-5106 |
| Year | 1998 |
| Author(s) | Antonio Abad, Consuelo Agulló, Manuel Arnó, Ana C. Cuñat, Benjamín Meseguer, Ramón J. Zaragozá |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo980311g |