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#18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL

Compound with spectra: 1 NMR, and 1 MS (GC)

#18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL
SpectraBase Compound ID JAEoVv7KTo2
InChI InChI=1S/C37H62O6Si/c1-25-19-28(41-23-39-9)20-27(31(25)42-24-40-10)21-37(38)26(2)13-14-29-33(6)17-18-36(43-44(11,12)32(3,4)5)22-35(36,8)30(33)15-16-34(29,37)7/h19-20,26,29-30,38H,13-18,21-24H2,1-12H3/t26-,29+,30+,33+,34+,35-,36+,37-/m0/s1
InChIKey VIZARAINWDZVNJ-KDBCUQKZSA-N
Mol Weight 631.0 g/mol
Molecular Formula C37H62O6Si
Exact Mass 630.431566 g/mol
Enantiomer InChIKey VIZARAINWDZVNJ-XOYKRBMRSA-N

View Spectrum of #18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL

MS (GC) Spectrum
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Source of Spectrum J-63-5106-18

View Spectrum of #18;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-ALPHA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • 1aS-(1a.alpha.,1b.beta.,3a.alpha.,4.alpha.,5.beta.,7a.beta.,7b.alpha.,9a.alpha.)]-9a-[(tert-Butyldimethylsilyl)oxy]-4-[(2,5-bis(methoxymethoxy)-3-methtylphenyl]methyl]-tetradecahydro-1a,3a,5,7b-tetramethyl-1H-cyclopropa[a]phenanthren-4-ol
#19;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,4-BETA,5-BETA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-4-[[2,5-BIS-(METHOXYMETHOXY)-3-METHYLPHENYL]
Title Journal or Book Year
An Efficient Stereoselective Synthesis of Stypodiol and Epistypodiol The Journal of Organic Chemistry 1998
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