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#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

Compound with spectra: 1 NMR, and 2 MS (GC)

#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA
SpectraBase Compound ID 7Zh5iwtABQk
InChI InChI=1S/C25H42O2Si/c1-17-10-11-18-22(5)14-15-25(27-28(8,9)21(2,3)4)16-24(25,7)19(22)12-13-23(18,6)20(17)26/h10,18-19H,11-16H2,1-9H3/t18-,19-,22-,23-,24+,25-/m1/s1
InChIKey RFSQYPXIKLPRFP-MDYXMDKASA-N
Mol Weight 402.7 g/mol
Molecular Formula C25H42O2Si
Exact Mass 402.295407 g/mol
Enantiomer InChIKey RFSQYPXIKLPRFP-BCZBAPJOSA-N

View Spectrum of #15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum F-55-12424-6

View Spectrum of #15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum J-63-5105-15

View Spectrum of #15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • [1aS-(1a.alpha.,1b.beta.,3a.alpha.,7a.beta.,7b.alpha.,9a.alpha.)]-9a-[(tert-Butyldimethylsilyl)oxy]-1,1a,1b,2,3,3a,7,7a,7b,8,9,9a-dodecahydro-1a,3a,5,7-tetramethyl-4H-cyclopropa[a]phenanthren-4-one
Lansioside-C,methylester, triacetate
2-ALPHA,11-BETA,13-TRIHYDROXYSTEMODANE
N-[4-benzoyl-1-(cyclohexylmethyl)-5-methyl-2-oxo-3-(trifluoromethyl)-2,3-dihydro-1H-pyrrol-3-yl]-3-(trifluoromethyl)benzamide
cis-(2R,3aR,4R,7aS)-2-(Phenylmethyl)-3-(2,2-dimethylethyl)-7,8,8-trimethyldecahydro-4a,7-methano-1H-1,3,2-oxazaphorinane-2-oxide
3-[(t-Butyldimethylsilyl)oxy]-15-benzyloxy-17-iodoandrosta-5,16-diene
1-tert-Butyl-2-methoxy-2H-pyridine-3,4,5,6-tetracarboxylic acid tetramethyl ester
1-PHENANTHRENECARBOXYLIC ACID, 6-AMINO-1,2,3,4,4a,9,10,10a-OCTAHYDRO-1,4a,-DIMETHYL-7-(1-METHYLETHYL)-8-NITRO- METHYL ESTER,
trans-(2S,3aR,4R,7aS)-2-(Phenylmethyl)-3-(2,2-dimethylethyl)-7,8,8-trimethyldecahydro-4a,7-methano-1H-1,3,2-oxazaphorinane-2-oxide
1,8-Diphenyl-15-oxahexaacyclo[6.6.1.1(2,5).1(4,7).0(2.7).0(9,14)]heptadeca-9,11,13-triene
1,3,4,9,10,10a-Hexahydro-6-hydroxy-1,1-dimethyl-7-(methylethyl)-2H-9,4a-(epoxymethano)phenanthrene-5,6-dione
Title Journal or Book Year
An Efficient Stereoselective Synthesis of Stypodiol and Epistypodiol The Journal of Organic Chemistry 1998
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