For citations & permissions, please see: Citations & Permissions - Wiley Science Solutions*

*Links on SpectraBase are not permalinks.

#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

Compound with spectra: 1 NMR, and 2 MS (GC)

#15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA
SpectraBase Compound ID 7Zh5iwtABQk
InChI InChI=1S/C25H42O2Si/c1-17-10-11-18-22(5)14-15-25(27-28(8,9)21(2,3)4)16-24(25,7)19(22)12-13-23(18,6)20(17)26/h10,18-19H,11-16H2,1-9H3/t18-,19-,22-,23-,24+,25-/m1/s1
InChIKey RFSQYPXIKLPRFP-MDYXMDKASA-N
Mol Weight 402.7 g/mol
Molecular Formula C25H42O2Si
Exact Mass 402.295407 g/mol
Enantiomer InChIKey RFSQYPXIKLPRFP-BCZBAPJOSA-N

View Spectrum of #15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum F-55-12424-6

View Spectrum of #15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum J-63-5105-15

View Spectrum of #15;[1A-S-(1A-ALPHA,1B-BETA,3A-ALPHA,7A-BETA,7B-ALPHA,9A-ALPHA)]-9A-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,1A,1B,2,3,3A,7,7A,7B,8,9,9A-DODECAHYDRO-1A,3A,5,7B-TETRA

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • [1aS-(1a.alpha.,1b.beta.,3a.alpha.,7a.beta.,7b.alpha.,9a.alpha.)]-9a-[(tert-Butyldimethylsilyl)oxy]-1,1a,1b,2,3,3a,7,7a,7b,8,9,9a-dodecahydro-1a,3a,5,7-tetramethyl-4H-cyclopropa[a]phenanthren-4-one
Lansioside-C,methylester, triacetate
3-[(t-Butyldimethylsilyl)oxy]-15-benzyloxy-17-iodoandrosta-5,16-diene
1-tert-Butyl-2-methoxy-2H-pyridine-3,4,5,6-tetracarboxylic acid tetramethyl ester
1,8-Diphenyl-15-oxahexaacyclo[6.6.1.1(2,5).1(4,7).0(2.7).0(9,14)]heptadeca-9,11,13-triene
1-PHENANTHRENECARBOXYLIC ACID, 6-AMINO-1,2,3,4,4a,9,10,10a-OCTAHYDRO-1,4a,-DIMETHYL-7-(1-METHYLETHYL)-8-NITRO- METHYL ESTER,
trans-(2S,3aR,4R,7aS)-2-(Phenylmethyl)-3-(2,2-dimethylethyl)-7,8,8-trimethyldecahydro-4a,7-methano-1H-1,3,2-oxazaphorinane-2-oxide
cis-(2R,3aR,4R,7aS)-2-(Phenylmethyl)-3-(2,2-dimethylethyl)-7,8,8-trimethyldecahydro-4a,7-methano-1H-1,3,2-oxazaphorinane-2-oxide
1,3,4,9,10,10a-Hexahydro-6-hydroxy-1,1-dimethyl-7-(methylethyl)-2H-9,4a-(epoxymethano)phenanthrene-5,6-dione
(4bR,8aR)-9-benzyl-6,7,8,9-tetrahydro-5H-8a,4b-(epoxyethano)carbazole
HKTWRGLIRIBFJB-UHFFFAOYSA-N
Title Journal or Book Year
An Efficient Stereoselective Synthesis of Stypodiol and Epistypodiol The Journal of Organic Chemistry 1998
Other Resources
Unknown Identification

Search your unknown spectrum against the world's largest collection of reference spectra

KnowItAll Campus Solutions

KnowItAll offers faculty and students at your school access to all the tools you need for spectral analysis and structure drawing & publishing! Plus, access the world's largest spectral library.