| SpectraBase Spectrum ID |
glCgD9TWc9 |
| Name |
3,4-Methylenedioxy-α-pyrrolidinohexanophenone |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 16361 |
| Lot Number |
Free base of 0464802-22 |
| Accessory |
DurasamplIR II |
| Acronyms |
3,4-MD-α-PHP; 3,4-MDPHP |
| Apodization Function |
Triangular |
| Copyright |
Copyright © 2019-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C17H23NO3 |
| IUPAC Name |
1-(1,3-Benzodioxol-5-yl)-2-(1-pyrrolidinyl)-1-hexanone |
| InChI |
InChI=1S/C17H23NO3/c1-2-3-6-14(18-9-4-5-10-18)17(19)13-7-8-15-16(11-13)21-12-20-15/h7-8,11,14H,2-6,9-10,12H2,1H3 |
| InChIKey |
OBLFRFGUZZRECT-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS
|
| SMILES |
c12c(ccc(c2)C(=O)C(N2CCCC2)CCCC)OCO1 |
| Sample Preparation Comments |
The HCl salt was dissolved in 0.5 mL water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 mL dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Scan Speed (number) |
5 |
| Solvent |
Dichloromethane |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film |
