SpectraBase Spectrum ID |
Z0Wwij0arW |
Name |
Cyclizine |
Source of Sample |
Spectrum Chemical Manufacturing Corp. |
Catalog Number |
Free base of C2986 |
Lot Number |
Free base of YM0010 |
Accessory |
DurasamplIR II |
CAS Registry Number |
82-92-8 |
Copyright |
Copyright © 2009-2024 John Wiley & Sons, Inc. All Rights Reserved. |
Formula |
C18H22N2 |
InChI |
InChI=1S/C18H22N2/c1-19-12-14-20(15-13-19)18(16-8-4-2-5-9-16)17-10-6-3-7-11-17/h2-11,18H,12-15H2,1H3 |
InChIKey |
UVKZSORBKUEBAZ-UHFFFAOYSA-N |
Instrument Name |
Bio-Rad FTS |
Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
Source of Spectrum |
Forensic Spectral Research |
Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |