SpectraBase Spectrum ID |
PlbInZBIcc |
Name |
N,N,N',N'-Tetramethyl-p-phenylenediamine |
Source of Sample |
Sigma-Aldrich Company Llc |
Catalog Number |
Free base of T3134 |
Lot Number |
Free base of 42F-0316 |
Accessory |
DurasamplIR II |
CAS Registry Number |
100-22-1 |
Copyright |
Copyright © 2014-2024 John Wiley & Sons, Inc. All Rights Reserved. |
Formula |
C10H16N2 |
InChI |
InChI=1S/C10H16N2/c1-11(2)9-5-7-10(8-6-9)12(3)4/h5-8H,1-4H3 |
InChIKey |
CJAOGUFAAWZWNI-UHFFFAOYSA-N |
Instrument Name |
Bio-Rad FTS |
Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
Source of Spectrum |
Forensic Spectral Research |
Synonyms |
Wurster's blue; TMPD |
Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |