| SpectraBase Spectrum ID |
LTlvqQlSavm |
| Name |
Quinacrine |
| Source of Sample |
Sigma-Aldrich Inc. |
| Catalog Number |
Free base of Q-0250 |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
83-89-6 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C23H30ClN3O |
| InChI |
InChI=1S/C23H30ClN3O/c1-5-27(6-2)13-7-8-16(3)25-23-19-11-9-17(24)14-22(19)26-21-12-10-18(28-4)15-20(21)23/h9-12,14-16H,5-8,13H2,1-4H3,(H,25,26) |
| InChIKey |
GPKJTRJOBQGKQK-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
