| SpectraBase Spectrum ID |
IdJtu09PqpO |
| Name |
Clomiphene |
| Source of Sample |
Spectrum Chemical Manufacturing Corp. |
| Catalog Number |
Free base of C1521 |
| Lot Number |
Free base of XO3120 |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
911-45-5 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2025 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C26H28ClNO |
| InChI |
InChI=1S/C26H28ClNO/c1-3-28(4-2)19-20-29-24-17-15-22(16-18-24)25(21-11-7-5-8-12-21)26(27)23-13-9-6-10-14-23/h5-18H,3-4,19-20H2,1-2H3 |
| InChIKey |
GKIRPKYJQBWNGO-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The citrate salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
