| SpectraBase Spectrum ID |
HpaVtljA4IV |
| Name |
Chloropseudoephedrine/Chloroephedrine |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 9002346 |
| Lot Number |
Free base of 0468756-5 |
| Accessory |
DurasamplIR II |
| Apodization Function |
Triangular |
| Comments |
mixture of diastereomers |
| Copyright |
Copyright © 2019-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C10H14ClN |
| InChI |
InChI=1S/C10H14ClN/c1-8(12-2)10(11)9-6-4-3-5-7-9/h3-8,10,12H,1-2H3/t8-,10?/m0/s1 |
| InChIKey |
HZCQDJZPLJOGQS-PEHGTWAWSA-N |
| Instrument Name |
Bio-Rad FTS
|
| SMILES |
N([C@](C(c1ccccc1)Cl)(C)[H])C |
| Sample Preparation Comments |
The HCl salt was dissolved in 0.5 mL water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 mL dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Scan Speed (number) |
5 |
| Solvent |
Dichloromethane |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film |
