| SpectraBase Spectrum ID |
F823hpTu35v |
| Name |
2,4-Dimethyl-1H-benzo[b][1,4]diazepine |
| Source of Sample |
Sigma-Aldrich Inc. |
| Catalog Number |
Free base of S3282-5 |
| Accessory |
DurasamplIR II |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C12H17N2 |
| InChI |
InChI=1S/C11H12N2/c1-8-7-9(2)13-11-6-4-3-5-10(11)12-8/h3-7,12H,1-2H3 |
| InChIKey |
GRSQZGQYBQLHAW-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
![2,4-Dimethyl-1H-benzo[b][1,4]diazepine](/api/spectrum/F823hpTu35v/structure.png?h=300&w=458 "2,4-Dimethyl-1H-benzo[b][1,4]diazepine")
