| SpectraBase Spectrum ID |
Epw5YMoXNUd |
| Name |
Primethixene |
| Source of Sample |
Sigma-Aldrich Inc. |
| Catalog Number |
Free base of P4545 |
| Lot Number |
Free base of 117F0852 |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
314-03-4 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2025 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C19H19NS |
| InChI |
InChI=1S/C19H19NS/c1-20-12-10-14(11-13-20)19-15-6-2-4-8-17(15)21-18-9-5-3-7-16(18)19/h2-9H,10-13H2,1H3 |
| InChIKey |
NZLVRVYNQYGMAB-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The maleate salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
