SpectraBase Spectrum ID |
E72btQHi1af |
Name |
Brompheniramine |
Source of Sample |
Spectrum Chemical Manufacturing Corp. |
Catalog Number |
Free base of BR167 |
Lot Number |
Free base of XS3035 |
Accessory |
DurasamplIR II |
CAS Registry Number |
86-22-6 |
Compound Type |
Pure |
Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
Formula |
C16H19BrN2 |
InChI |
InChI=1S/C16H19BrN2/c1-19(2)12-10-15(16-5-3-4-11-18-16)13-6-8-14(17)9-7-13/h3-9,11,15H,10,12H2,1-2H3 |
InChIKey |
ZDIGNSYAACHWNL-UHFFFAOYSA-N |
Instrument Name |
Bio-Rad FTS |
Sample Preparation Procedure |
The maleate salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
Source of Spectrum |
Forensic Spectral Research |
Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |