| SpectraBase Spectrum ID |
DEFsH4L94an |
| Name |
Chlordiazepoxide |
| Source of Sample |
Sigma-Aldrich, Inc. |
| Catalog Number |
Free base of C-2517 |
| Lot Number |
Free base of 94H1023 |
| CAS Registry Number |
58-25-3 |
| Comments |
white crystals |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C16H14ClN3O |
| InChI |
InChI=1S/C16H14ClN3O/c1-18-15-10-20(21)16(11-5-3-2-4-6-11)13-9-12(17)7-8-14(13)19-15/h2-9H,10H2,1H3,(H,18,19) |
| InChIKey |
ANTSCNMPPGJYLG-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. The solvent was evaporated from the tube using a flow of nitrogen gas. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
KBr0 |
