| SpectraBase Spectrum ID |
CUsTRscvjxA |
| Name |
4-Bromopyridine |
| Source of Sample |
Sigma-Aldrich Inc. |
| Catalog Number |
Free base of B80429 |
| Lot Number |
Free base of 02508MX |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
1120-87-2 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C5H4BrN |
| InChI |
InChI=1S/C5H4BrN/c6-5-1-3-7-4-2-5/h1-4H |
| InChIKey |
BSDGZUDFPKIYQG-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Neat (DuraSamplIR II) Film? |
