| SpectraBase Spectrum ID |
CDSp7TV2XV1 |
| Name |
Robenidine |
| Source of Sample |
Riedel-De Haen Vetranal, Sigma-Aldrich Inc. |
| Catalog Number |
Free base of 33979 |
| Lot Number |
Free base of 7145X |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
25875-51-8 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2025 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C15H13Cl2N5 |
| InChI |
InChI=1S/C15H13Cl2N5/c16-13-5-1-11(2-6-13)9-19-21-15(18)22-20-10-12-3-7-14(17)8-4-12/h1-10H,(H3,18,21,22)/b19-9+,20-10+ |
| InChIKey |
MOOFYEJFXBSZGE-LQGKIZFRSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
