Wiley SpectraBase; SpectraBase Compound ID=HdiGtsPw9d SpectraBase Spectrum ID=BcIXkKdaaFw
http://spectrabase.com/spectrum/BcIXkKdaaFw (accessed Aug 12, 2020).

1-(4-Methylphenyl)piperazine 2HCl
SpectraBase Compound ID HdiGtsPw9d
InChI InChI=1S/C11H16N2.2ClH/c1-10-2-4-11(5-3-10)13-8-6-12-7-9-13;;/h2-5,12H,6-9H2,1H3;2*1H
InChIKey PMGFOTNCJZITIM-UHFFFAOYSA-N
Mol Weight 249.19 g/mol
Molecular Formula C11H18Cl2N2
Exact Mass 248.084704 g/mol

Attenuated Total Reflectance Infrared (ATR-IR) Spectrum

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Attenuated Total Reflectance Infrared (ATR-IR) Spectrum

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SpectraBase Spectrum ID BcIXkKdaaFw
SpectraBase Batch ID EuaNQSND8h6
Name 1-(4-Methylphenyl)piperazine 2HCl
Source of Sample Sigma-Aldrich Inc.
Catalog Number HCl salt of 71868
Lot Number HCl salt of 1425262
Accessory DurasamplIR II
CAS Registry Number 13078-14-3
Compound Type Pure
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Formula C11H18Cl2N2
InChI InChI=1S/C11H16N2.2ClH/c1-10-2-4-11(5-3-10)13-8-6-12-7-9-13;;/h2-5,12H,6-9H2,1H3;2*1H
InChIKey PMGFOTNCJZITIM-UHFFFAOYSA-N
Instrument Name Bio-Rad FTS
Sample Preparation Procedure The free amine was added to a test tube, and a minimum amount of dichloromethane (several drops) was added to completely dissolve the sample. The test tube was then filled halfway with anhydrous diethyl ether or hexane. Hydrochloric acid gas was bubbled through the solution, which led to the precipitation of the HCl salt of amine. The test tube was spun in a centrifuge to separate the HCl salt precipitate from the organic solvent. The organic solvent was removed from the tube, and the precipitate was dried with nitrogen gas.
Source of Spectrum Forensic Spectral Research
SpectraBase Compound ID HdiGtsPw9d
Technique ATR-Neat (DuraSamplIR II)