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6-exo-(tert-butyldimethylsilyloxymethyl)-3-exo/endo-isopropyl-cis-perhydro-furo[2,3-b]pyran
SpectraBase Compound ID AVUlbcEFcEK
InChI InChI=1S/C17H34O3Si/c1-12(2)15-11-18-16-14(15)9-8-13(20-16)10-19-21(6,7)17(3,4)5/h12-16H,8-11H2,1-7H3/t13-,14-,15?,16-/m0/s1
InChIKey RIXPLIDNSQUMRF-OJTCVJSUSA-N
Mol Weight 314.5 g/mol
Molecular Formula C17H34O3Si
Exact Mass 314.227721 g/mol

Mass Spectrum (GC)

Mass Spectrum (GC)

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SpectraBase Spectrum ID 9rXeTyaX9hj
Name 6-exo-(tert-butyldimethylsilyloxymethyl)-3-exo/endo-isopropyl-cis-perhydro-furo[2,3-b]pyran
Appearance Colourless oil
Carrier Gas Helium (1.4 ml/min)
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Exact Mass 314.227721487 u
Formula C17H34O3Si
GC Column Macherey-Nagel Optima delta-3 (20 m x 0.25 mm, film thickness 0.25 micrometer)
GC Oven Program Oven temp 280oC
InChI InChI=1S/C17H34O3Si/c1-12(2)15-11-18-16-14(15)9-8-13(20-16)10-19-21(6,7)17(3,4)5/h12-16H,8-11H2,1-7H3/t13-,14-,15?,16-/m0/s1
InChIKey RIXPLIDNSQUMRF-OJTCVJSUSA-N
Inlet Type Split
Instrument Name Finnigan Trace GC/MS
Ionization Type EI
Literature Reference DOI 10.1002/anie.201604950
Molecular Weight 314.541 g/mol
Quality 157
Reported Formula C17H34O3Si
SMILES C(O[Si](C(C)(C)C)(C)C)[C@]1(O[C@]2([C@@](CC1)(C(CO2)C(C)C)[H])[H])[H]
SPLASH splash10-004i-9430000000-51b6a919c36202d65a15
Sample Comments Major, dr = 2:1
Source of Spectrum ACI-55-SM12-9b (DOI: 10.1002/anie.201604950)
Wiley ID 1899228