Wiley SpectraBase; SpectraBase Compound ID=HdiGtsPw9d SpectraBase Spectrum ID=9cnUhliDu2G
http://spectrabase.com/spectrum/9cnUhliDu2G (accessed Aug 09, 2020).

1-(4-Methylphenyl)piperazine 2HCl
SpectraBase Compound ID HdiGtsPw9d
InChI InChI=1S/C11H16N2.2ClH/c1-10-2-4-11(5-3-10)13-8-6-12-7-9-13;;/h2-5,12H,6-9H2,1H3;2*1H
InChIKey PMGFOTNCJZITIM-UHFFFAOYSA-N
Mol Weight 249.19 g/mol
Molecular Formula C11H18Cl2N2
Exact Mass 248.084704 g/mol

Transmission Infrared (IR) Spectrum

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Transmission Infrared (IR) Spectrum

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SpectraBase Spectrum ID 9cnUhliDu2G
SpectraBase Batch ID BGGsYXFat22
Name 1-(4-Methylphenyl)piperazine 2HCl
Source of Sample Sigma-Aldrich, Inc.
Catalog Number HCl salt of 71868
Lot Number HCl salt of 0001425262
CAS Registry Number 13078-14-3
Copyright Copyright © 2012-2020 John Wiley & Sons, Inc. All Rights Reserved.
Formula C11H18Cl2N2
InChI InChI=1S/C11H16N2.2ClH/c1-10-2-4-11(5-3-10)13-8-6-12-7-9-13;;/h2-5,12H,6-9H2,1H3;2*1H
InChIKey PMGFOTNCJZITIM-UHFFFAOYSA-N
Instrument Name Bio-Rad FTS
Sample Preparation Procedure The free amine was added to a test tube, and a minimum amount of dichloromethane (several drops) was added to completely dissolve the sample. The test tube was then filled halfway with anhydrous diethyl ether or hexane. Hydrochloric acid gas was bubbled through the solution, which led to the precipitation of the HCl salt of amine. The test tube was spun in a centrifuge to separate the HCl salt precipitate from the organic solvent. The organic solvent was removed from the tube, and the precipitate was dried with nitrogen gas.
Source of Spectrum Forensic Spectral Research
SpectraBase Compound ID HdiGtsPw9d
Technique KBr0P