SpectraBase Spectrum ID |
9TmqPCUXuwW |
Name |
Phendimetrazine |
Source of Sample |
Alltech Associates, Inc., Grace Davison Discovery Sciences |
Catalog Number |
Free base of 01774 |
Lot Number |
Free base of 48A |
Accessory |
DurasamplIR II |
CAS Registry Number |
634-03-7 |
Compound Type |
Pure |
Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
Formula |
C12H17NO |
InChI |
InChI=1S/C12H17NO/c1-10-12(14-9-8-13(10)2)11-6-4-3-5-7-11/h3-7,10,12H,8-9H2,1-2H3 |
InChIKey |
MFOCDFTXLCYLKU-UHFFFAOYSA-N |
Instrument Name |
Bio-Rad FTS |
Sample Preparation Procedure |
The bitartrate salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
Source of Spectrum |
Forensic Spectral Research |
Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |