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2ALPHA-OXO-2BETA-METHOXY-3ALPHA-HYDROXY-3BETA-PHENYL-5,5-DIMETHYL-1,2-OXAPHOSPHOLANE
SpectraBase Compound ID EsTk9GwHrBB
InChI InChI=1S/C12H17O4P/c1-11(2)9-12(13,17(14,15-3)16-11)10-7-5-4-6-8-10/h4-8,13H,9H2,1-3H3/t12-,17+/m1/s1
InChIKey JKIJFJNSTJKOOS-PXAZEXFGSA-N
Mol Weight 256.24 g/mol
Molecular Formula C12H17O4P
Exact Mass 256.086446 g/mol

31P Nuclear Magnetic Resonance (NMR) Chemical Shifts

31P Nuclear Magnetic Resonance (NMR) Chemical Shifts

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SpectraBase Spectrum ID 9TavSNhNMPQ
Name 2ALPHA-OXO-2BETA-METHOXY-3ALPHA-HYDROXY-3BETA-PHENYL-5,5-DIMETHYL-1,2-OXAPHOSPHOLANE
Comments , C=0.3M. `+` AXIS-LOW FIELD (DIRECT INDICATION IN THE ARTICLE).
Copyright Copyright © 2002-2024 Wiley-VCH Verlag GmbH & Co. KGaA. All Rights Reserved.
Formula C12H17O4P
InChI InChI=1S/C12H17O4P/c1-11(2)9-12(13,17(14,15-3)16-11)10-7-5-4-6-8-10/h4-8,13H,9H2,1-3H3/t12-,17+/m1/s1
InChIKey JKIJFJNSTJKOOS-PXAZEXFGSA-N
Instrument Name Jeol FX-60
Literature Reference ANDRZEJ E. WROBLEWSKI (1986) Phosphorus and Sulfur: v.28, N3, 371-377.
NMR Standard H3PO4 85%
Observed nucleus 31P
Origin Chemical Concepts. A Wiley Division. Weinheim, Germany
Solvent CH4O methanol