| SpectraBase Spectrum ID |
9DM158SuW3e |
| Name |
(+/-)-threo-4-Methylmethylphenidate |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 35030 |
| Lot Number |
Free base of 0661429-4 |
| Accessory |
DurasamplIR II |
| Apodization Function |
Norton-Beer, medium |
| Copyright |
Copyright © 2019-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C15H21NO2 |
| InChI |
InChI=1S/C15H21NO2/c1-11-6-8-12(9-7-11)14(15(17)18-2)13-5-3-4-10-16-13/h6-9,13-14,16H,3-5,10H2,1-2H3/t13-,14-/m0/s1 |
| InChIKey |
WJZNCJIOIACDBR-KBPBESRZSA-N |
| Instrument Name |
Bio-Rad FTS |
| SMILES |
N1[C@@](CCCC1)([C@@](C(OC)=O)(c1ccc(C)cc1)[H])[H] |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 mL water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 mL dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film in the diamond window for ATR-IR. |
| Solvent |
Dichloromethane |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film |
