| SpectraBase Spectrum ID |
94ML7rePi2e |
| Name |
1-Ethyl-5-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one |
| Source of Sample |
Maybridge, Part of Thermo Fisher Scientific |
| Catalog Number |
Free base of NRB00843 |
| Accessory |
DurasamplIR II |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C12H16N2O |
| InChI |
InChI=1S/C12H16N2O/c1-3-14-11-7-5-4-6-10(11)13(2)9-8-12(14)15/h4-7H,3,8-9H2,1-2H3 |
| InChIKey |
HERCTTZSBHLIOW-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
