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2BETA-OXO-2ALPHA-METHOXY-3BETA-(TERT-BUTYLDIMETHYLSILYLOXY)-4BETA-HYDROXY-5BETA-HYDROXYMETHYL-1,2-OXAPHOSPHOLANE, 4,5-O-BENZYLIDENE
SpectraBase Compound ID 2GO5559bZw1
InChI InChI=1S/C18H29O6PSi/c1-18(2,3)26(5,6)24-17-15-14(23-25(17,19)20-4)12-21-16(22-15)13-10-8-7-9-11-13/h7-11,14-17H,12H2,1-6H3/t14-,15+,16+,17-,25-/m1/s1
InChIKey KNZHKXOSGWSYJF-GHDLQHMGSA-N
Mol Weight 400.48 g/mol
Molecular Formula C18H29O6PSi
Exact Mass 400.147102 g/mol

31P Nuclear Magnetic Resonance (NMR) Chemical Shifts

31P Nuclear Magnetic Resonance (NMR) Chemical Shifts

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SpectraBase Spectrum ID 8V5SsSF8AuM
Name 2BETA-OXO-2ALPHA-METHOXY-3BETA-(TERT-BUTYLDIMETHYLSILYLOXY)-4BETA-HYDROXY-5BETA-HYDROXYMETHYL-1,2-OXAPHOSPHOLANE, 4,5-O-BENZYLIDENE
Comments , C=0.3M. `+` AXIS-LOW FIELD (DIRECT INDICATION IN THE ARTICLE).
Copyright Copyright © 2002-2024 Wiley-VCH Verlag GmbH & Co. KGaA. All Rights Reserved.
Formula C18H29O6PSi
InChI InChI=1S/C18H29O6PSi/c1-18(2,3)26(5,6)24-17-15-14(23-25(17,19)20-4)12-21-16(22-15)13-10-8-7-9-11-13/h7-11,14-17H,12H2,1-6H3/t14-,15+,16+,17-,25-/m1/s1
InChIKey KNZHKXOSGWSYJF-GHDLQHMGSA-N
Instrument Name Jeol FX-60
Literature Reference ANDRZEJ E. WROBLEWSKI (1986) Phosphorus and Sulfur: v.28, N3, 371-377.
NMR Standard H3PO4 85%
Observed nucleus 31P
Origin Chemical Concepts. A Wiley Division. Weinheim, Germany
Solvent CHCl3 chloroform