| SpectraBase Spectrum ID |
8R2gxcP0SgJ |
| Name |
Bromhexine |
| Source of Sample |
Spectrum Chemical Manufacturing Corp. |
| Catalog Number |
Free base of B1552 |
| Lot Number |
Free base of XV3102 |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
3572-43-8 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C14H20Br2N2 |
| InChI |
InChI=1S/C14H20Br2N2/c1-18(12-5-3-2-4-6-12)9-10-7-11(15)8-13(16)14(10)17/h7-8,12H,2-6,9,17H2,1H3 |
| InChIKey |
OJGDCBLYJGHCIH-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
