| SpectraBase Spectrum ID |
7znIYnK8uUt |
| Name |
Methiothepin |
| Source of Sample |
Sigma-Aldrich Company Llc |
| Catalog Number |
Free base of M149 |
| Lot Number |
Free base of 123M4719V |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
20229-30-5 |
| Classification |
serotonin receptor antagonist, which blocks serotonin autoreceptors |
| Copyright |
Copyright © 2014-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C20H24N2S2 |
| InChI |
InChI=1S/C20H24N2S2/c1-21-9-11-22(12-10-21)18-13-15-5-3-4-6-19(15)24-20-8-7-16(23-2)14-17(18)20/h3-8,14,18H,9-13H2,1-2H3 |
| InChIKey |
RLJFTICUTYVZDG-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The mesylate salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Synonyms |
1-[10,11-Dihydro-8-(methylthio)dibenzo[b,f]thiepin-10-yl]-4-methylpiperazine |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
