| SpectraBase Spectrum ID |
7mFaT9nUD1H |
| Name |
3,4-Trimethylene-α-piperidinovalerophenone |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 37751 |
| Lot Number |
Free base of 0665044-2 |
| Accessory |
DurasamplIR II |
| Apodization Function |
Norton-Beer, medium |
| Copyright |
Copyright © 2019-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C19H27NO |
| InChI |
InChI=1S/C19H27NO/c1-2-7-18(20-12-4-3-5-13-20)19(21)17-11-10-15-8-6-9-16(15)14-17/h10-11,14,18H,2-9,12-13H2,1H3 |
| InChIKey |
XCBQKBNQNYAXPN-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| SMILES |
c1c(ccc2CCCc12)C(C(N1CCCCC1)CCC)=O |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 mL water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 mL dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film in the diamond window for ATR-IR. |
| Solvent |
Dichloromethane |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film |
