SpectraBase Spectrum ID |
5f0Dft5NN21 |
Name |
2,3-MDA |
Source of Sample |
Cayman Chemical Company |
Catalog Number |
Free base of 13969 |
Lot Number |
Free base of 0444081-5 |
Accessory |
DurasamplIR II |
CAS Registry Number |
23693-17-6 |
Classification |
psychedelic and entactogenic drug that is scheduled as a controlled substance in the United States |
Copyright |
Copyright © 2014-2024 John Wiley & Sons, Inc. All Rights Reserved. |
Formula |
C10H13NO2 |
InChI |
InChI=1S/C10H13NO2/c1-7(11)5-8-3-2-4-9-10(8)13-6-12-9/h2-4,7H,5-6,11H2,1H3 |
InChIKey |
XOOVOZRNDZPGLF-UHFFFAOYSA-N |
Instrument Name |
Bio-Rad FTS |
Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
Source of Spectrum |
Forensic Spectral Research |
Synonyms |
2,3-Methylenedioxyamphetamine |
Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |