| SpectraBase Spectrum ID |
53JGKfTj3Cx |
| Name |
3,4-Methylenedioxy-α-pyrrolidinobutiophenone |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 10437 |
| Lot Number |
Free base of 0471746-1 |
| Accessory |
DurasamplIR II |
| Acronyms |
3,4-MDPBP |
| Apodization Function |
Triangular |
| Copyright |
Copyright © 2019-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C15H19NO3 |
| IUPAC Name |
1-(1,3-Benzodioxol-5-yl)-2-(1-pyrrolidinyl)-1-butanone |
| InChI |
InChI=1S/C15H19NO3/c1-2-12(16-7-3-4-8-16)15(17)11-5-6-13-14(9-11)19-10-18-13/h5-6,9,12H,2-4,7-8,10H2,1H3 |
| InChIKey |
OLVLMDVPMCIBQW-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS
|
| SMILES |
c12c(ccc(c2)C(C(CC)N2CCCC2)=O)OCO1 |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 mL water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 mL dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Scan Speed (number) |
5 |
| Solvent |
Dichloromethane |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film |
