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2,3,4,5-Tetrahydro-1H-1,4-benzodiazepine HCl
SpectraBase Compound ID EiZ5JzvdW7T
InChI InChI=1S/C9H12N2.ClH/c1-2-4-9-8(3-1)7-10-5-6-11-9;/h1-4,10-11H,5-7H2;1H
InChIKey GJEJQSFAQPMOOD-UHFFFAOYSA-N
Mol Weight 184.67 g/mol
Molecular Formula C9H13ClN2
Exact Mass 184.076726 g/mol

Attenuated Total Reflectance Infrared (ATR-IR) Spectrum

Attenuated Total Reflectance Infrared (ATR-IR) Spectrum

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SpectraBase Spectrum ID 4qdVnHccMRl
Name 2,3,4,5-Tetrahydro-1H-1,4-benzodiazepine HCl
Source of Sample Enamine Ltd
Catalog Number HCl salt of EN300-39371
Lot Number HCl salt of R439163
Accessory DurasamplIR II
Compound Type Pure
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Formula C9H13ClN2
InChI InChI=1S/C9H12N2.ClH/c1-2-4-9-8(3-1)7-10-5-6-11-9;/h1-4,10-11H,5-7H2;1H
InChIKey GJEJQSFAQPMOOD-UHFFFAOYSA-N
Instrument Name Bio-Rad FTS
Sample Preparation Procedure The free amine was added to a test tube, and a minimum amount of dichloromethane (several drops) was added to completely dissolve the sample. The test tube was then filled halfway with anhydrous diethyl ether or hexane. Hydrochloric acid gas was bubbled through the solution, which led to the precipitation of the HCl salt of amine. The test tube was spun in a centrifuge to separate the HCl salt precipitate from the organic solvent. The organic solvent was removed from the tube, and the precipitate was dried with nitrogen gas.
Source of Spectrum Forensic Spectral Research
Technique ATR-Neat (DuraSamplIR II)