| SpectraBase Spectrum ID |
4ixwd6epQgg |
| Name |
2,3-Dichlorophenylpiperazine |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 14296 |
| Lot Number |
Free base of 0446497-1 |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
41202-77-1 |
| Classification |
precursor in the synthesis of aripiprazole and one of its metabolites |
| Copyright |
Copyright © 2014-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C10H12Cl2N2 |
| InChI |
InChI=1S/C10H12Cl2N2/c11-8-2-1-3-9(10(8)12)14-6-4-13-5-7-14/h1-3,13H,4-7H2 |
| InChIKey |
UDQMXYJSNNCRAS-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Synonyms |
2,3-DCPP; 1-(2,3-Dichlorophenyl)-piperazine |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
