| SpectraBase Spectrum ID |
4dCX0CFPwbg |
| Name |
3-Bromo-α-pyrrolidinovalerophenone |
| Source of Sample |
Cayman Chemical Company |
| Catalog Number |
Free base of 37631 |
| Lot Number |
Free base of 0663548-3 |
| Accessory |
DurasamplIR II |
| Apodization Function |
Norton-Beer, medium |
| Copyright |
Copyright © 2019-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C15H20BrNO |
| InChI |
InChI=1S/C15H20BrNO/c1-2-6-14(17-9-3-4-10-17)15(18)12-7-5-8-13(16)11-12/h5,7-8,11,14H,2-4,6,9-10H2,1H3 |
| InChIKey |
HDRJPUUDIBCDBJ-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| SMILES |
c1(cccc(c1)C(C(CCC)N1CCCC1)=O)Br |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 mL water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 mL dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film in the diamond window for ATR-IR. |
| Solvent |
Dichloromethane |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film |
