| SpectraBase Spectrum ID |
3bLCYq5DQEf |
| Name |
Pyrilamine |
| Source of Sample |
Sigma-Aldrich Company Llc |
| Catalog Number |
Free base of P5514 |
| Lot Number |
Free base of SLBC1954V |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
91-84-9 |
| Classification |
histamine |
| Copyright |
Copyright © 2014-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C17H23N3O |
| InChI |
InChI=1S/C17H23N3O/c1-19(2)12-13-20(17-6-4-5-11-18-17)14-15-7-9-16(21-3)10-8-15/h4-11H,12-14H2,1-3H3 |
| InChIKey |
YECBIJXISLIIDS-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The maleate salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Synonyms |
Mepyramine: N-(4-Methoxyphenyl)methyl-N′,N′-dimethyl-N-(2-pyridinyl)-1,2-ethanediamine |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
