| SpectraBase Spectrum ID |
2bEJGsGZOUI |
| Name |
(cis/trans) Dothiepin |
| Source of Sample |
Lipomed AG |
| Catalog Number |
Free base of DOT-1337-HC |
| Lot Number |
Free base of 1337.1B0.1 |
| Accessory |
DurasamplIR II |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C19H21NS |
| InChI |
InChI=1S/C19H21NS/c1-20(2)13-7-11-17-16-9-4-3-8-15(16)14-21-19-12-6-5-10-18(17)19/h3-6,8-12H,7,13-14H2,1-2H3 |
| InChIKey |
PHTUQLWOUWZIMZ-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Synonyms |
3-Dibenzo[b,e]thepin-11(6H)-ylidine-N,N-dimethyl-1-propanamine |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
