SpectraBase Spectrum ID |
2Jiz2AB0mIN |
Name |
L-N-Methylephedrine |
Source of Sample |
Alltech Associates, Inc., Grace Davison Discovery Sciences |
Catalog Number |
Free base of 01644 |
Lot Number |
Free base of 478 |
Accessory |
DurasamplIR II |
CAS Registry Number |
552-79-4 |
Copyright |
Copyright © 2009-2025 John Wiley & Sons, Inc. All Rights Reserved. |
Formula |
C11H17NO |
InChI |
InChI=1S/C11H17NO/c1-9(12(2)3)11(13)10-7-5-4-6-8-10/h4-9,11,13H,1-3H3/t9-,11-/m0/s1 |
InChIKey |
FMCGSUUBYTWNDP-ONGXEEELSA-N |
Instrument Name |
Bio-Rad FTS |
Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
Source of Spectrum |
Forensic Spectral Research |
Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |