| SpectraBase Spectrum ID |
1IaHmEppt8L |
| Name |
Loperamide |
| Source of Sample |
Riedel-De Haen Vetranal, Sigma-Aldrich Inc. |
| Catalog Number |
Free base of 34014 |
| Lot Number |
Free base of 6108X |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
53179-11-6 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C29H33ClN2O2 |
| InChI |
InChI=1S/C29H33ClN2O2/c1-31(2)27(33)29(24-9-5-3-6-10-24,25-11-7-4-8-12-25)19-22-32-20-17-28(34,18-21-32)23-13-15-26(30)16-14-23/h3-16,34H,17-22H2,1-2H3 |
| InChIKey |
RDOIQAHITMMDAJ-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
