Bio-Rad Laboratories, Inc. SpectraBase; SpectraBase Compound ID=kfGQEdISs SpectraBase Spectrum ID=13JAO56PoEq
http://spectrabase.com/spectrum/13JAO56PoEq (accessed May 25, 2020).

19-(S)-BrOMO-17-BETA-(TERT.-BUTYLDIMETHYLSILYLOXY)-5-BETA,6-BETA-DIBrOMOMETHYLENE-9-ALPHA,19-CYClO-10-ALPHA-ANDROSTAN-3-ONE
SpectraBase Compound ID kfGQEdISs
InChI InChI=1S/C26H39Br3O2Si/c1-21(2,3)32(5,6)31-19-8-7-16-17-13-18-25(26(18,28)29)14-15(30)9-10-24(25)20(27)23(17,24)12-11-22(16,19)4/h16-20H,7-14H2,1-6H3/t16-,17-,18+,19-,20-,22-,23-,24+,25+/m0/s1
InChIKey KPYPESPHTMZQOL-IBYXANEBSA-N
Mol Weight 651.4 g/mol
Molecular Formula C26H39Br3O2Si
Exact Mass 648.026942 g/mol

13C Nuclear Magnetic Resonance (NMR) Chemical Shifts

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SpectraBase Spectrum ID 13JAO56PoEq
SpectraBase Batch ID JZAJ9Qp2fU2
Name 19(S)-bromo-17-β-(tert-butyl-dimethylsiloxy)-5-β,6-β-dibromomethylene-9-α,19-cyclo-10-α-androstan-3-one
Comments original value for tert.-Bu: 2.84 ppm changed to 28.4 ppm /sv/28.10.99
Compound Number 8B
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InChI InChI=1S/C26H39Br3O2Si/c1-21(2,3)32(5,6)31-19-8-7-16-17-13-18-25(26(18,28)29)14-15(30)9-10-24(25)20(27)23(17,24)12-11-22(16,19)4/h16-20H,7-14H2,1-6H3/t16-,17-,18+,19-,20-,22-,23-,24+,25+/m0/s1
InChIKey KPYPESPHTMZQOL-IBYXANEBSA-N
Literature Reference J.F.TEMPLETON,Y.LING,W.LIN,R.J.PITURA,K.MARAT,J.N.BRIDSON J.CHEM.SOC.PERKIN-1,1149(1994)
Solvent Methanol-d4
Technique SELECTIVE DECOUPLING; C/H SHIFT CORRELATION