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6,6'-Bis(diethoxyphosphoryl)-1,1'-binaphthalene-2,2'-diyl bis(methanesulfonate)

Compound with spectra: 2 NMR, and 1 MS (GC)

6,6'-Bis(diethoxyphosphoryl)-1,1'-binaphthalene-2,2'-diyl bis(methanesulfonate)
SpectraBase Compound ID lccO1jsT2K
InChI InChI=1S/C30H36O12P2S2/c1-7-37-43(31,38-8-2)23-13-15-25-21(19-23)11-17-27(41-45(5,33)34)29(25)30-26-16-14-24(44(32,39-9-3)40-10-4)20-22(26)12-18-28(30)42-46(6,35)36/h11-20H,7-10H2,1-6H3
InChIKey YOWUAKICPMMDGO-UHFFFAOYSA-N
Mol Weight 714.7 g/mol
Molecular Formula C30H36O12P2S2
Exact Mass 714.112343 g/mol

View Spectrum of 6,6'-Bis(diethoxyphosphoryl)-1,1'-binaphthalene-2,2'-diyl bis(methanesulfonate)

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of 6,6'-Bis(diethoxyphosphoryl)-1,1'-binaphthalene-2,2'-diyl bis(methanesulfonate)

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum KC-1-2087-8

View Spectrum of 6,6'-Bis(diethoxyphosphoryl)-1,1'-binaphthalene-2,2'-diyl bis(methanesulfonate)

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
2,2'-DIACETYL-1,1'-BINAPHTHYL-6,6'-BIS-(DIETHYLPHOSPHONATE)
6,6'-BIS-(DIETHOXYPHOSPHORYL)-1,1'-BINAPHTHALENE-2,2'-DIYLDIPENTANOATE
6-Phenyl-2,2'-dipivaloyloxy-1,1'-binaphthyl
6-((1-Phenyl)-ethyn-2-yl)-2,2'-dipivaloyloxy-1,1'-binaphthyl
6-Vinyl-2,2'-dipivaloyloxy-1,1'-binaphthyl
2-Trifluoromethanesulfonyloxy-7,7'-dibromo-2'-hydroxy-1.1'-binaphthalene
2,2'-(1,1'-Binaphthalene-2,2'-diyloxy)bis(ethyl) bis(toluene-4-sulfonate)
(R)-BIPHENYL-XU-PHOS
[1-(2-methoxynaphthalen-1-yl)naphthalen-2-yl]-di(phenyl)phosphane
O,O'-[(R)-1,1'-Binaphthalene-2,2'-diyl] N-Benzyl-N-[(R)-1-phenylethyl]phosphoramidite
Title Journal or Book Year
Phosphonation of 1,1′-binaphthalene-2,2′-diol (BINOL): synthesis of (R)- and (S )-2,2′-dihydroxy-1,1′-binaphthalene-6,6′-diyldiphosphonic acid Journal of the Chemical Society, Perkin Transactions 1 1998

This compound is available in the following databases:

Wiley Registry of Mass Spectral Data 2023
Author: Wiley

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