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4-N-[5'-O-(4,4'-DIMETHOXYTRITYL)-THYMIDINE-3'-YL]-(2-CYANOETHYL)-PHOSPHORYL-3',5'-O-BIS-(TERT.-BUTYLDIMETHYLSILYL)-DEOXYCYTIDINE

Compound with spectra: 2 NMR

4-N-[5'-O-(4,4'-DIMETHOXYTRITYL)-THYMIDINE-3'-YL]-(2-CYANOETHYL)-PHOSPHORYL-3',5'-O-BIS-(TERT.-BUTYLDIMETHYLSILYL)-DEOXYCYTIDINE
SpectraBase Compound ID KtvimbMdoDh
InChI InChI=1S/C55H75N6O13PSi2/c1-37-34-61(52(64)58-50(37)62)49-32-43(45(71-49)35-68-55(38-18-15-14-16-19-38,39-20-24-41(66-8)25-21-39)40-22-26-42(67-9)27-23-40)73-75(65,69-31-17-29-56)59-47-28-30-60(51(63)57-47)48-33-44(74-77(12,13)54(5,6)7)46(72-48)36-70-76(10,11)53(2,3)4/h14-16,18-28,30,34,43-46,48-49H,17,31-33,35-36H2,1-13H3,(H,58,62,64)(H,57,59,63,65)/t43-,44-,45+,46+,48+,49+,75?/m0/s1
InChIKey MJJZRMIROXOYIG-NLOUAAAASA-N
Mol Weight 1115.4 g/mol
Molecular Formula C55H75N6O13PSi2
Exact Mass 1114.466827 g/mol
Enantiomer InChIKey MJJZRMIROXOYIG-KDCQMQEWSA-N

View Spectrum of 4-N-[5'-O-(4,4'-DIMETHOXYTRITYL)-THYMIDINE-3'-YL]-(2-CYANOETHYL)-PHOSPHORYL-3',5'-O-BIS-(TERT.-BUTYLDIMETHYLSILYL)-DEOXYCYTIDINE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of 4-N-[5'-O-(4,4'-DIMETHOXYTRITYL)-THYMIDINE-3'-YL]-(2-CYANOETHYL)-PHOSPHORYL-3',5'-O-BIS-(TERT.-BUTYLDIMETHYLSILYL)-DEOXYCYTIDINE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
#4AB;FAST;N-[5'-O-(4,4'-DIMETHOXYTRITYL)-3'-AMINO-3'-DEOXYTHYMIDIN-3'-YL]-O-[N-(4)-BENZOYL-3'-O-TERT.-BUTYLDIMETHYLSILYL-2'-DEOXYCYTIDIN-5'-YL]-METHANEPHOSPHO
#5B;(R)-N-ACETYL-2-PYRROLIDINYLMETHYL-N4-(BENZOYL)-5'-O-(PARA,PARA'-DIMETHOXYTRITYL)-2'-DEOXYCYTIDIN-3'-YL-3'-O-(TERT.-BUTYLDIMETHYLSILYL)-THYMIDIN-5'-YL-(R)-P
#6B;(S)-N-ACETYL-2-PYRROLIDINYLMETHYL-N4-(BENZOYL)-5'-O-(PARA,PARA'-DIMETHOXYTRITYL)-2'-DEOXYCYTIDIN-3'-YL-3'-O-(TERT.-BUTYLDIMETHYLSILYL)-THYMIDIN-5'-YL-(S)-P
#4BA;FAST;N-[N-(4)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-AMINO-2'.3'-DIDEOXYCYTIDIN-3'-YL]-O-(3'-O-TERT.-BUTYLDIMETHYLSILYLTHYMIDIN-5'-YL)-METHANEPHOSPHONAMI
5'-O-DIMETHOXYTRITYL-3'-O-TERT.-BUTYLDIPHENYLSILYL-ALPHA,BETA-D-CNA-TT-(RC,RP)
CEWNGWIAOJUILI-BMERVDLTSA-N
#10;5'-O-[BIS-(4-METHOXYPHENYL)-(PHENYL)-METHYL]-3'-O-[(2-CYANOETHOXY)-[2-(4,5-DIHYDRO-3,4-DIMETHYL-2-OXO-5-PHENYL-[1,3,2]-OXAZAPHOSPHOL-2-YL)-ETHYL]-PHOSPHINO
3'-O-ACETYL-5'-(5'-O-TRITYLDEOXYTHYMIDINE-3'-N,N'-DICYCLOHEXYLUREIDOAMIDOPHOSPHORYL)DEOXYTHYMIDINE (DIASTEREOMER MIXTURE)
5'-O-(DIMETHOXYTRITYL)-3'-(O-TERT.-BUTYLDIMETHYLSILYL)-2'-DEOXY-2'-ALPHA-C-[N-(5'-DEOXYTHYMIDINE-5-YL)-CARBAMOYLMETHYL]-URIDINE
#29;N-BENZOYL-5-METHYL-[3'-O-[2-CYANOETHYL-(DIISOPROPYLAMINO)-PHOSPHANYL]-5'-O-(4,4'-DIMETHOXYTRITYL)-2'-O-(2-TRIFLUOROACETAMIDO)-ETHYL-BETA-D-RIBOFURANOSYL]-C
Title Journal or Book Year
Proton-Block Strategy for the Synthesis of Oligodeoxynucleotides without Base Protection, Capping Reaction, and P−N Bond Cleavage Reaction The Journal of Organic Chemistry 2003
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