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5-ACETYL-5,7A-DIHYDRO-7-(TERT.-BUTYL)-SPIRO-[3H-1,2,4-DIAZA-1-PHOSPHOLO]-[4,3-C]-[1,2,3]-DIAZAPHOSPHOLE-3,9'-[9H]-FLUORENE

Compound with spectra: 2 NMR, and 1 MS (GC)

5-ACETYL-5,7A-DIHYDRO-7-(TERT.-BUTYL)-SPIRO-[3H-1,2,4-DIAZA-1-PHOSPHOLO]-[4,3-C]-[1,2,3]-DIAZAPHOSPHOLE-3,9'-[9H]-FLUORENE
SpectraBase Compound ID JNRrlbHctLq
InChI InChI=1S/C21H21N4OP/c1-13(26)25-23-18(20(2,3)4)19-22-24-21(27(19)25)16-11-7-5-9-14(16)15-10-6-8-12-17(15)21/h5-12,19H,1-4H3
InChIKey LUHIUBDQNBEEFF-UHFFFAOYSA-N
Mol Weight 376.4 g/mol
Molecular Formula C21H21N4OP
Exact Mass 376.145298 g/mol

View Spectrum of 5-ACETYL-5,7A-DIHYDRO-7-(TERT.-BUTYL)-SPIRO-[3H-1,2,4-DIAZA-1-PHOSPHOLO]-[4,3-C]-[1,2,3]-DIAZAPHOSPHOLE-3,9'-[9H]-FLUORENE

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of 5-ACETYL-5,7A-DIHYDRO-7-(TERT.-BUTYL)-SPIRO-[3H-1,2,4-DIAZA-1-PHOSPHOLO]-[4,3-C]-[1,2,3]-DIAZAPHOSPHOLE-3,9'-[9H]-FLUORENE

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum AJ-43-357-6

View Spectrum of 5-ACETYL-5,7A-DIHYDRO-7-(TERT.-BUTYL)-SPIRO-[3H-1,2,4-DIAZA-1-PHOSPHOLO]-[4,3-C]-[1,2,3]-DIAZAPHOSPHOLE-3,9'-[9H]-FLUORENE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • 5-Acetyl-5,7a-dihydro-7-(t-butyl)-spiro[3H-1,2,4-diazaphospholo[4,3-c]-(1,2,3)-diazaphosphole-3,9'-[9H}-fluorene
Title Journal or Book Year
1,3-Dipolar cycloadditions of 9-diazofluorenes and diphenyldiazomethane to 2-acyl-2H-1,2,3-diazaphospholes Journal of Heterocyclic Chemistry 2006
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