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(+/-)-(1-ALPHA,2-ALPHA,5-ALPHA)-2-AZIDO-2-([(TERT.-BUTYLDIPHENYLSILYL)-OXY]-METHYL)-6-OXABICYCLO-[3.1.0]-HEXANE

Compound with spectra: 1 NMR

(+/-)-(1-ALPHA,2-ALPHA,5-ALPHA)-2-AZIDO-2-([(TERT.-BUTYLDIPHENYLSILYL)-OXY]-METHYL)-6-OXABICYCLO-[3.1.0]-HEXANE
SpectraBase Compound ID I1x95HCzrue
InChI InChI=1S/C22H27N3O2Si/c1-21(2,3)28(17-10-6-4-7-11-17,18-12-8-5-9-13-18)26-16-22(24-25-23)15-14-19-20(22)27-19/h4-13,19-20H,14-16H2,1-3H3/t19-,20-,22-/m1/s1
InChIKey ATQIKZIXVRILKY-KCZVDYSFSA-N
Mol Weight 393.56 g/mol
Molecular Formula C22H27N3O2Si
Exact Mass 393.187254 g/mol
Enantiomer InChIKey ATQIKZIXVRILKY-ONTIZHBOSA-N

View Spectrum of (+/-)-(1-ALPHA,2-ALPHA,5-ALPHA)-2-AZIDO-2-([(TERT.-BUTYLDIPHENYLSILYL)-OXY]-METHYL)-6-OXABICYCLO-[3.1.0]-HEXANE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
(3R,4S)-4,5-Bis(benzyloxy)-3-(tert-butyldiphenylsilyloxymethyl)-3-hydroxypentanenitrile
(2R,3S)-1,4-DI-O-TERT.-BUTYLDIPHENYLSILYL-3-O-BENZYL-2-ETHYLBUTANE-1,2,3,4-TETRAOL
1,7-Dioxaspiro[5.5]undecane-2-ethanol, 8-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]-.beta.,3,9-trimethyl-, [2S-[2.alpha.(S*),3.alpha.,6.beta.(8S*,9S*)]]-
(-)-(7R,8R,10S)-10-[(tert-butyldiphenylsilyloxy)methyl]-8-methyl-1,4-dioxaspiro[4.5]decan-7-ol
(-)-(7S,8S,10S)-10-[(tert-butyl-diphenylsilyloxy)methyl]-8-methyl-1,4-dioxaspiro[4.5]decan-7-ol
3-BENZYLOXYMETHYL-2-[2-(TERT.-BUTYLDIPHENYLSILANYLOXY)-1-METHYL-ETHYL]-4-METHYLENE-CYCLOPENTANOL
(2S,3S)-2-[[tert-butyl(diphenyl)silyl]oxymethyl]-3-hydroxy-1-piperidinecarboxylic acid tert-butyl ester
3-O-Benzyl-2,4-di-O-benzylidene-1-O-(t-butyldiphenylsilyl)butane-1,2,3,4-tetrol
(1S,2R,3R,4R)-2-(TERT.-BUTYLDIPHENYLSILYLOXYMETHYL)-1,4-DI-O-(TRIETHYLSILYL)-3-ETHYL-CYCLOPENTANE-1,4-DIOL
SM-8-60
Title Journal or Book Year
An allylic azide route to 4'-azido carbocyclic nucleosides. Synthesis of (.+-.)-(1'.alpha.,2'.alpha.,3'.beta.)- and (.+-.)-(1'.alpha.,2'.beta.,3'.beta.)-1-[1-azido-2-hydroxy-1-(hydroxymethyl)-3-cyclopentyl]thymine The Journal of Organic Chemistry 1992
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