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[(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MAJOR-PRODUCT

Compound with spectra: 4 NMR

[(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MAJOR-PRODUCT
SpectraBase Compound ID HQQlbNT8I8z
InChI InChI=1S/C28H28NO2PSSi/c1-23-28(24-15-7-3-8-16-24)30-32(33,29(23)2)31-34(25-17-9-4-10-18-25,26-19-11-5-12-20-26)27-21-13-6-14-22-27/h3-23,28H,1-2H3/t23-,28-,32?/m0/s1
InChIKey GJKUISRILOQUEO-MIQQLYACSA-N
Mol Weight 501.66 g/mol
Molecular Formula C28H28NO2PSSi
Exact Mass 501.134764 g/mol
Enantiomer InChIKey GJKUISRILOQUEO-YPWQLUCXSA-N

View Spectrum of [(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MAJOR-PRODUCT

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent C6D6

View Spectrum of [(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MAJOR-PRODUCT

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent C6D6

View Spectrum of [(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MAJOR-PRODUCT

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent C6D6

View Spectrum of [(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MAJOR-PRODUCT

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent C6D6
  • [(1R,2S)-EPHEDRINE]-P(=S)OSIPH3;MINOR-PRODUCT
(2R,4S,5S)-3,4-Dimethyl-2-((3-methyl-1,5-cyclohexenyl-1-oxy)-5-phenyl-1,3,2-oxazaphospholidin-2-one
(2R,4S,5R)-3,4-Dimethyl-2-((3-methyl-1,5-cyclohexenyl-1-oxy)-5-phenyl-1,3,2-oxazaphospholidin-2-one
(2R,4S,5R)-2-(1-BENZYLOXYIMINOETHYL)-3,4-DIMETHYL-2-OXO-5-PHENYL-2-LAMBDA5-1,3,2-OXAZAPHOSPHOLIDINE
(2S,4S,5R)-2-(1-BENZYLOXYIMINOETHYL)-3,4-DIMETHYL-2-OXO-5-PHENYL-2-LAMBDA5-1,3,2-OXAZAPHOSPHOLIDINE
NZGJJTLHGOTBAE-JLMWTWJWSA-N
1-[5-O-(tert-BUTYL-DIPHENYLSILYL)-2,3-DIDEOXY-beta-D-GLYCERO-PENTO-2-ENOFURANOSYL)-THYMINE
Ethyl 2-methyl-5-phenylthieno[3,2-b]thiophene-3-carboxylate
1-((1R,2R,3R)-TETRAHYDRO-2-HYDROXY-3-((1,1-DIMETHYLETHYLDIPHENYL)-SILYLOXY)-METHYL)-1-FURANYL)-2,4(1H,3H)-PYRIMIDINEDIONE
(5S,6R)-2-sec-Butyl-2-hydroxy-4,5-dimethyl-6-phenylmorpholin-3-one
2-{[4-(4-chlorophenyl)-5-(3-methylphenyl)-4H-1,2,4-triazol-3-yl]sulfanyl}-N-(3-methoxyphenyl)acetamide
Title Journal or Book Year
Synthetic, stereochemical and mechanistic studies on the asymmetric phosphonylation of aldehydes via 2-triorganosiloxy-1,3,2-oxazaphospholidines Journal of the Chemical Society, Perkin Transactions 1 1993
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