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4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

Compound with spectra: 5 NMR, and 4 MS (GC)

4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide
SpectraBase Compound ID FlM1ElSjDdt
InChI InChI=1S/C5H9O4P/c1-5-2-7-10(6,8-3-5)9-4-5/h2-4H2,1H3
InChIKey SEOXVQTUPVKLTH-UHFFFAOYSA-N
Mol Weight 164.1 g/mol
Molecular Formula C5H9O4P
Exact Mass 164.023846 g/mol

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

MS (GC) Spectrum
Copyright Copyright © 2002-2024 Wiley-VCH Verlag GmbH & Co. KGaA. All Rights Reserved.
Source of Spectrum Chemical Concepts, A Wiley Division, Weinheim, Germany

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum W5-1989-32596-1

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum O-15-521-2

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

17O NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent TOLUENE

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

17O NMR Spectrum
Copyright Copyright © 2002-2024 Wiley-VCH Verlag GmbH & Co. KGaA. All Rights Reserved.
Solvent Acetone

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of 4-Methyl-2,6,7-trioxa-1-phosphabicyclo-[2.2.2]-octane-1-oxide

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • 1,3-Propanediol, 2-(hydroxymethyl)-2-methyl-, cyclic phosphate
1,3-Propanediol, 2,2-dimethyl-, cyclic hydrogen phosphate
5,5-Dimethyl-2-oxo-1,3,2-dioxaphosphorinane-2-selenol anion
2,2-Dimethylpropyl ethyl methyl phosphate
1,3,2-Dioxaphosphorinane, 2,5,5-trimethyl-, 2-oxide
2A-FLUORO-2E-OXO-5,5-DIMETHYL-1,3,2-DIOXAPHOSPHORINANE
2-Chloro-5,5-dimethyl-1,3,2-dioxaphosphorinan-2-one
2-AMINO-2-OXO-5,5-DIMETHYL-1,3,2-DIOXAZAPHOSPHORINAN
1,3-Propanediol, 2-ethyl-2-(hydroxymethyl)-, mono(dihydrogen phosphate)
2-(2-HYDROXYETHOXY)-2-OXO-1,3,2-DIOXAPHOSPHORINANE
2-THIOXO-2-HYDROXY-5,5-DIMETHYL-1,3,2-DIOXAPHOSPHORINANE
Title Journal or Book Year
Methanolysis of 4-Methyl-2,6,7-trioxa-1-phospha-bicyclo[2.2.2]octane 1-Oxide and 1-Sulfide: Mechanistic and Stereochemical Considerations Australian Journal of Chemistry 1994
Oxygen-17 NMR spectra of cyclic phosphites, phosphates, and thiophosphates Journal of the American Chemical Society 1986
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