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(TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

Compound with spectra: 15 NMR

(TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]
SpectraBase Compound ID B7JzDrh8qrF
InChI InChI=1S/C22H17F12O2P/c1-2-3-12-37(15-10-6-4-8-13(15)17(35-37,19(23,24)25)20(26,27)28)16-11-7-5-9-14(16)18(36-37,21(29,30)31)22(32,33)34/h4-11H,2-3,12H2,1H3
InChIKey HKTLODXGGNHOGC-UHFFFAOYSA-N
Mol Weight 572.33 g/mol
Molecular Formula C22H17F12O2P
Exact Mass 572.077455 g/mol

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

19F NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

19F NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

19F NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

19F NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

19F NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent TOLUENE-D8

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent ET2O

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent ET2O

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent THF

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent TOLUENE-D8

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (TBPY-5-12)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • [TBPY-5-11]-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[1,3-DIHYDRO-2,1-LAMBDA-5-BENZOXAPHOSPHOLE]
  • [TBPY-5-12]-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[1,3-DIHYDRO-2,1-LAMBDA-5-BENZOXAPHOSPHOLE]
  • HKTLODXGGNHOGC-UHFFFAOYSA-N
  • [TBPY-5-12]-1-N-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H,2,1,5-LAMBDA-BENZOXAPHOSPHOLE]
  • [TBPY-5-11]-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H,2,1,LAMBDA(5)-BENZOXAPHOSPHOLE]
  • [TBPY-5-12]-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H,2,1,LAMBDA(5)-BENZOXAPHOSPHOLE]
(TBPY-5-11)-1-BUTYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H-2,1-(5)-LAMBDA-BENZOXAPHOSPHOLE]
[TBPY-5-11]-1-(2,6-DIMETHYL-4-METHOXY)-PHENYL-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[3H,2,1,LAMBDA(5)-BENZOXAPHOSPHOLE]
[TBPY-5-11]-1-(1,1-DIMETHYLETHYL)-3,3,3',3'-TETRAKIS-(TRIFLUOROMETHYL)-1,1'-SPIROBI-[1,3-DIHYDRO-2,1-LAMBDA-5-BENZOXAPHOSPHOLE]
HPSUJIRGGCGFDQ-UHFFFAOYSA-N
9-methylsulfanyl-7,7,7',7'-tetrakis(trifluoromethyl)-9,9'-spirobi[8-oxa-9$l^{5}-phosphabicyclo[4.3.0]nona-1,3,5-triene]
Spiro[3,5-dioxatricyclo[6.3.0.0(2,7)]undecan-6-one-4,2'-cyclohexane], 9,11-dihydroxy-1'-isopropyl-2,4'-dimethyl-
Estra-1,3,5(10),9(11)-tetraen-17-one, 1,4-dimethoxy-14-methyl-
10-Amino-6-oxo-6H-dibenzo[c,h]chromene-8,9-dicarboxylic acid diethyl ester
OCTAMETHYL-TRILOBATIN-C
Spiro-[Fluoreno[4,3-b]pyran-2(7H)-,9'(9H)-thioxanthene
Title Journal or Book Year
Characteristic Reactions and Properties of C-Apical O-Equatorial (O-cis) Spirophosphoranes:  Effect of the σ*P-O Orbital in the Equatorial Plane and Isolation of a Hexacoordinate Oxaphosphetane as an Intermediate of the Wittig Type Reaction of 10-P-5 Phosphoranes Journal of the American Chemical Society 2002
Highly Selective One-Pot Synthesis of Spirophosphoranes Exhibiting Reversed Apicophilicity by Oxidation of Dianions Generated from P−H Spirophosphorane Organic Letters 2001
First Characterization of a 10-P-5 Spirophosphorane with an Apical Carbon−Equatorial Oxygen Ring. Kinetic Studies on Pseudorotation of Stereoisomers Journal of the American Chemical Society 1996
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