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[(3A'S,4'R,5'R,6A'R)-4'-ALLYL-5,5-DIMETHYLHEXAHYDRO-1'H-SPIRO-[1,3-DIOXANE-2,2'-PENTALEN]-5'-YL]-OXY]-(TERT.-BUTYL)-DIPHENYLSILANE

Compound with spectra: 1 NMR

[(3A'S,4'R,5'R,6A'R)-4'-ALLYL-5,5-DIMETHYLHEXAHYDRO-1'H-SPIRO-[1,3-DIOXANE-2,2'-PENTALEN]-5'-YL]-OXY]-(TERT.-BUTYL)-DIPHENYLSILANE
SpectraBase Compound ID 73ew2VBJkgY
InChI InChI=1S/C32H44O3Si/c1-7-14-27-28-21-32(33-22-31(5,6)23-34-32)20-24(28)19-29(27)35-36(30(2,3)4,25-15-10-8-11-16-25)26-17-12-9-13-18-26/h7-13,15-18,24,27-29H,1,14,19-23H2,2-6H3/t24-,27-,28+,29-/m1/s1
InChIKey RQICABSUAPAILK-DAUHHZGYSA-N
Mol Weight 504.8 g/mol
Molecular Formula C32H44O3Si
Exact Mass 504.305972 g/mol
Enantiomer InChIKey RQICABSUAPAILK-IMYHUDGHSA-N

View Spectrum of [(3A'S,4'R,5'R,6A'R)-4'-ALLYL-5,5-DIMETHYLHEXAHYDRO-1'H-SPIRO-[1,3-DIOXANE-2,2'-PENTALEN]-5'-YL]-OXY]-(TERT.-BUTYL)-DIPHENYLSILANE

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
(1R,3AS,4R,5R,6AS)-1,4-DIALLYL-5-[(TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-HEXAHYDROPENTALEN-2(1H)-ONE
(1S,3AS,5R,6R,6AS)-1,6-DIALLYL-5-[(TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-HEXAHYDROPENTALEN-2(1H)-ONE
[[(3AS,5R,6R,6AS)-6-ALLYL-5-[[TERT.-BUTYL-(DIPHENYL)-SILYL]-OXY]-1,3A,4,5,6,6A-HEXAHYDROPENTALEN-2-YL]-OXY]-(TRIETHYL)-SILANE
5'-(t-Butyldimethylsilyloxy)-[4'-(2-N-methyl-S-phenylsulfonimidoyl)ethenyl]-octahydro-5,5-dimethyl-spiro[1,3-dioxan-2,2(1'H)-pentalene]}
(5E,1R*,2R*,4S*,8S*)-1-[(tert-Butyldimethylsilyl)oxy[-5-(cyclohexylmethylene)-2-[(phentlsilyl)methyl]bicyclo[4.3.0]nonane
1-(3"-Acetyloxy-1"-octenyl)-5-[(1',1'-dimethylethyl)diphenylsilyloxy]octahydro-2-pentalenyl benzoate
(1S)-1-(3"-Hydroxy-1"-octenyl)-5-[(1',1'-dimethylethyl)diphenylsilyloxy]octahydro-2-pentalenyl benzoate
(4'R)-Hexahydro-4'-(1"-heptenyl)-2',2',5,5-tetramethylspiro[1,3-dioxane-2,6'(5'H)-4'H-pentaleno[2,1-d]-(1,3)-dioxine
5-[(1',1'-Dimethylethyl)diphenylsilyloxy]hexahydro-1-(1''-triethylsilyloxy-2"-octenyl)-2(1H)-pentalenone
(1R,3S,4S,5R)-3-[tert-butyl(diphenyl)silyl]oxy-4-methyl-5-(4-nitrophenyl)sulfonyloxy-1-cyclohexanecarboxylic acid methyl ester
Title Journal or Book Year
Doing it Twice: Asymmetric Deprotonation/Alkylation of Weiss Diketone Derivatives as Key Steps in the Functionalization of Bicyclo[3.3.0]octanes European Journal of Organic Chemistry 2012
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