For citations & permissions, please see: Citations & Permissions - Wiley Science Solutions*

*Links on SpectraBase are not permalinks.

2-[(1-Phenylsulfonyl)tryptophyl]-4-(tert-butoxycarbonyl)-5-cyano-6-methoxy-7-(trimethylsiloxy)-1,2,5,6,7,8,9,10-octahydroisoquinoline

Compound with spectra: 1 NMR, and 1 MS (GC)

2-[(1-Phenylsulfonyl)tryptophyl]-4-(tert-butoxycarbonyl)-5-cyano-6-methoxy-7-(trimethylsiloxy)-1,2,5,6,7,8,9,10-octahydroisoquinoline
SpectraBase Compound ID 68gZ1BR4kX9
InChI InChI=1S/C35H45N3O6SSi/c1-35(2,3)43-34(39)29-23-37(21-25-19-31(44-46(5,6)7)33(42-4)28(20-36)32(25)29)18-17-24-22-38(30-16-12-11-15-27(24)30)45(40,41)26-13-9-8-10-14-26/h8-16,22-23,25,28,31-33H,17-19,21H2,1-7H3/t25-,28+,31-,32+,33-/m1/s1
InChIKey SSHHNDYIAAYAJQ-INRYUVOSSA-N
Mol Weight 663.9 g/mol
Molecular Formula C35H45N3O6SSi
Exact Mass 663.279834 g/mol
Enantiomer InChIKey SSHHNDYIAAYAJQ-GAOBKBBCSA-N

View Spectrum of 2-[(1-Phenylsulfonyl)tryptophyl]-4-(tert-butoxycarbonyl)-5-cyano-6-methoxy-7-(trimethylsiloxy)-1,2,5,6,7,8,9,10-octahydroisoquinoline

MS (GC) Spectrum
Copyright Copyright © 2020-2024 John Wiley & Sons, Inc. All Rights Reserved.
Source of Spectrum C-112-7690-29

View Spectrum of 2-[(1-Phenylsulfonyl)tryptophyl]-4-(tert-butoxycarbonyl)-5-cyano-6-methoxy-7-(trimethylsiloxy)-1,2,5,6,7,8,9,10-octahydroisoquinoline

13C NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
1H-Indole, 3-[[2-(1H-indol-3-yl)-4,6-dimethyl-3-cyclohexen-1-yl]carbonyl]-1-[(4-methylphenyl)sulfonyl]-, (1.alpha.,2.beta.,6.beta.)-(.+-.)-
(5-ETA-C5H5)-TICL2-[N-P-(TERT.-BUTYL)2-(2-CH2-PY)]
17.alpha.-(1,3-Dihydro-2H-inden-5-yl)-estradiol
Methyl 3,7-Diethyl-6-(4-methoxyphenyl)-2,3,6,7-tetrahydro-1H-azocino[5,4-b]indole-5-carboxylate
24(.xi.)-methylcholest-5-ene-1.alpha.,3.beta.,11.alpha.-triol
ethyl 4-(6-chloro-1,3-benzodioxol-5-yl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydro-3-quinolinecarboxylate
Diindolyl-methane compound of yohimbine (isomer 1)
isobutyl 4-[2-(benzyloxy)phenyl]-7-(4-chlorophenyl)-2-methyl-5-oxo-1,4,5,6,7,8-hexahydro-3-quinolinecarboxylate
Cholic acid tetra(trimethylsilyl) ester
Cholic acid, 4TMS
Title Journal or Book Year
Formal total synthesis of deserpidine demonstrating a versatile amino-Claisen rearrangement/Wenkert cyclization strategy for the preparation of functionalized yohimbane ring systems Journal of the American Chemical Society 1990
Other Resources
Unknown Identification

Search your unknown spectrum against the world's largest collection of reference spectra

KnowItAll Campus Solutions

KnowItAll offers faculty and students at your school access to all the tools you need for spectral analysis and structure drawing & publishing! Plus, access the world's largest spectral library.