For citations & permissions, please see: Citations & Permissions - Wiley Science Solutions*

*Links on SpectraBase are not permalinks.

(RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE

Compound with spectra: 2 NMR

(RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE
SpectraBase Compound ID 3UlZztNDSdC
InChI InChI=1S/C35H42N3O6PSi/c1-25-22-38(34(40)36-33(25)39)32-21-29(43-45-37(5)23-30(44-45)26-15-9-6-10-16-26)31(42-32)24-41-46(35(2,3)4,27-17-11-7-12-18-27)28-19-13-8-14-20-28/h6-20,22,29-32H,21,23-24H2,1-5H3,(H,36,39,40)/t29-,30+,31+,32+,45?/m1/s1
InChIKey SZIITLCFBCDMHB-RVZBIXSSSA-N
Mol Weight 659.8 g/mol
Molecular Formula C35H42N3O6PSi
Exact Mass 659.25805 g/mol
Enantiomer InChIKey SZIITLCFBCDMHB-GKTBEPTLSA-N

View Spectrum of (RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • (SP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE
(SP)-5'-O-[BIS-(4-METHOXYPHENYL)-PHENYLMETHYL]-3'-O-[(2S,5S)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE
5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[2-(3-NITROBENZAMIDO)-ETHOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE;FAST-DIASTEREOMER
#28;5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[2-[N-ISOPROPYL-N-(4-METHOXYBENZOYL)-AMINO]-ETHOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE;FAST-DIASTEREOMER
5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[2-(BENZAMIDO)-2-METHYLPROPOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE;FAST-DIASTEREOMER
3'-O-ACETYL-5'-(5'-O-ANILIDOPHOSPHORYLDEOXYTHYMIDIN-3'-YLOXY(ANILIDO)PHOSPHORYL)DEOXYTHYMIDINE (DIASTEREOMER MIXTURE)
5'-O-(5'-TRITYLDEOXYTHYMIDINE-3'-BENZOYLPHOSPHORYL)DEOXYTHYMIDINE(DIASTEREOMER MIXTURE)
3'-O-ACETYL-5'-O-(5'-O-TRITYLDEOXYTHYMID-3'-YLOXY(4-NITROPHENYL)PHOSPHORYL)DEOXYTHYMIDINE (DIASTEREOMER MIXTURE)
5'-(3'-O-ACETYL-5'-N-CYCLOHEXYLAMIDOPHOSPHORYLDEOXYTHYMIDIN-3'-YLOXY(CYCLOHEXYLAMIDO)PHOSPHORYL)-3'-O-ACETYLDEOXYTHYMIDINE (DIASTEREOMERMIXTURE)
5'-O-METHOXYTRITYLDEOXYTHYMIDINE-3'-PHENYL(ANILIDO)PHOSPHATE(DIASTEREOMER MIXTURE)
3'-O-ACETYL-5'-O-(4,4'-DIMETHOXYTRITYL)-DITHYMIDYLYL-3',5'-PHOSPHOROTHIOSELENOATE
Title Journal or Book Year
An Oxazaphospholidine Approach for the Stereocontrolled Synthesis of Oligonucleoside Phosphorothioates Journal of the American Chemical Society 2003
Other Resources
Unknown Identification

Search your unknown spectrum against the world's largest collection of reference spectra

KnowItAll Campus Solutions

KnowItAll offers faculty and students at your school access to all the tools you need for spectral analysis and structure drawing & publishing! Plus, access the world's largest spectral library.