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(RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE

Compound with spectra: 2 NMR

(RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE
SpectraBase Compound ID 3UlZztNDSdC
InChI InChI=1S/C35H42N3O6PSi/c1-25-22-38(34(40)36-33(25)39)32-21-29(43-45-37(5)23-30(44-45)26-15-9-6-10-16-26)31(42-32)24-41-46(35(2,3)4,27-17-11-7-12-18-27)28-19-13-8-14-20-28/h6-20,22,29-32H,21,23-24H2,1-5H3,(H,36,39,40)/t29-,30+,31+,32+,45?/m1/s1
InChIKey SZIITLCFBCDMHB-RVZBIXSSSA-N
Mol Weight 659.8 g/mol
Molecular Formula C35H42N3O6PSi
Exact Mass 659.25805 g/mol
Enantiomer InChIKey SZIITLCFBCDMHB-GKTBEPTLSA-N

View Spectrum of (RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3

View Spectrum of (RP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE

31P NMR Spectrum
Copyright Copyright © 2016-2024 W. Robien, Inst. of Org. Chem., Univ. of Vienna. All Rights Reserved.
Solvent CDCl3
  • (SP)-5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-O-[(2R,5R)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE
(SP)-5'-O-[BIS-(4-METHOXYPHENYL)-PHENYLMETHYL]-3'-O-[(2S,5S)-3-METHYL-5-PHENYL-1,3,2-OXAZAPHOSPHOLIDIN-2-YL]-THYMIDINE
5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[2-(3-NITROBENZAMIDO)-ETHOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE;FAST-DIASTEREOMER
#28;5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[2-[N-ISOPROPYL-N-(4-METHOXYBENZOYL)-AMINO]-ETHOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE;FAST-DIASTEREOMER
5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[2-(BENZAMIDO)-2-METHYLPROPOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE;FAST-DIASTEREOMER
3'-O-ACETYL-5'-(5'-O-ANILIDOPHOSPHORYLDEOXYTHYMIDIN-3'-YLOXY(ANILIDO)PHOSPHORYL)DEOXYTHYMIDINE (DIASTEREOMER MIXTURE)
ALLYL-[5'-O-(PARA,PARA'-DIMETHOXYTRITYL)-THYMIDYLYL]-(3'-5')-[3'-O-(TERT.-BUTYLDIMETHYLSILYL)-THYMIDINE]
5'-O-(5'-TRITYLDEOXYTHYMIDINE-3'-BENZOYLPHOSPHORYL)DEOXYTHYMIDINE(DIASTEREOMER MIXTURE)
3'-O-ACETYL-5'-O-(5'-O-TRITYLDEOXYTHYMID-3'-YLOXY(4-NITROPHENYL)PHOSPHORYL)DEOXYTHYMIDINE (DIASTEREOMER MIXTURE)
5'-(3'-O-ACETYL-5'-N-CYCLOHEXYLAMIDOPHOSPHORYLDEOXYTHYMIDIN-3'-YLOXY(CYCLOHEXYLAMIDO)PHOSPHORYL)-3'-O-ACETYLDEOXYTHYMIDINE (DIASTEREOMERMIXTURE)
5'-O-METHOXYTRITYLDEOXYTHYMIDINE-3'-PHENYL(ANILIDO)PHOSPHATE(DIASTEREOMER MIXTURE)
Title Journal or Book Year
An Oxazaphospholidine Approach for the Stereocontrolled Synthesis of Oligonucleoside Phosphorothioates Journal of the American Chemical Society 2003
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